GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber

GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber

Conditions

sample/matrix white wine spiked with 50 ppb pesticides
desorption process 250 °C for 5 min
extraction immersion, room temp (30 min)
SPME fiber 85 µm polyacrylate (57304)
column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 60 °C (1 min), 15 °C/min to 100 °C, 7 °C/min to 300 °C (1 min)
carrier gas helium, 0.7 mL/min, constant
liner 0.75 mm I.D. SPME liner
MSD interface 325 °C
scan range SIM

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Food & Beverage Analysis, Pesticides, Foods, Flavors & Fragrances, Pesticide and Metabolite Residues, Beverage Testing, Applications (Chromatograms), Beer, Wine, and Spirits, Wine
Featured Industry Food and Beverages
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for SPME, application for GC

Analyte

  • 1-Naphthyl-N-methylcarbamate
  • Azinphos-methyl
  • Carbaryl
  • Chloropyrifos-methyl
  • Diazinon
  • Dichlofluanid
  • Dicloran
  • Dicofol
  • Methiocarb
  • Myclobutanil
  • Parathion
  • Phosalone
  • Procymidone
  • Triadimefon
  • Vinclozolin

Materials

     
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