GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) in Water on a 5% Phenyl Column after SPE using Supelclean™ ENVI-18

GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) in Water on a 5% Phenyl Column after SPE using Supelclean™ ENVI-18

Conditions

sample preparation SPE (Solid Phase Extraction)
sample/matrix water spiked with PAHs
SPE tube/cartridge Supelclean ENVI-18, 500 mg/6 mL (57064)
condition 2 x 6 mL toluene:methanol (10:1); 6 mL methanol; 6 mL DI water
sample addition 250 mL water sample at 10 mL/min
drying 10 min under vacuum
elution 2 x 1 mL toluene:methanol (10:1)
column 5% phenyl polysiloxane, 30m x 0.25 mm I.D., 0.25 µm film (Supelco equivalent, SLB-5ms, 28471-U)
oven 70 °C (2 min) to 280 °C at 8 °C/min
carrier gas helium
injection 1 µL
detector FID, 310 °C

Description

Categories Analytical Chromatography, Food & Beverage Analysis, SPE Applications, GC Applications, Phenols & Semivolatiles in water, Processing/Packaging Contaminants, PAHs, Hydrocarbons, Applications (Chromatograms)
Featured Industry Environmental
Food and Beverages
General description See "Related Products" to find associated products for sale.
For more information, email: Supelco Technical Service
Legal Information Supelclean is a trademark of Sigma-Aldrich Co. LLC
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suitability application for GC, application for SPE

Analyte

  • Acenaphthylene
  • Anthracene
  • Benzo[a]anthracene
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[ghi]perylene
  • Benzo[k]fluoranthene
  • Chrysene
  • Dibenzo[a,h]anthracene
  • Dibenzo[a,h]anthracene
  • Fluorene
  • Indeno[1,2,3-cd]pyrene
  • Indeno[1,2,3-cd]pyrene
  • Phenanthrene
  • Pyrene

Materials

     
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