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GC Analysis of Volatiles in Water on SPB®-1 after SPME using 100 μm PDMS Fiber

GC Analysis of Volatiles in Water on SPB®-1 after SPME using 100 μm PDMS Fiber

Conditions

extraction 5 min immersed in water with rapid stirring
SPME fiber polydimethylsiloxane, 100 µm (57300-U)
column SPB-1, 10 m x 0.20 mm I.D., 1.2 µm (24134-U)
oven 40 C ( 0.75 min) to 160 C at 20 C/min
carrier gas helium, 40 cm/sec
sample 50ppb each analyte in 1.8 mL saturated salt water
inj. temp. 230 C, splitless (closed 3 min)
detector FID, 260 C

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Volatiles
Featured Industry Environmental
Food and Beverages
Legal Information SPB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for SPME, application for GC

Analyte

  • 1,1,1-Trichloroethane
  • 1,1,2,2-Tetrachloroethane
  • 1,1,2-Trichloroethane
  • 1,1-Dichloroethane
  • 1,1-Dichloroethylene
  • 1,2-Dichlorobenzene
  • 1,2-Dichloroethane
  • 1,2-Dichloropropane
  • 1,3-Dichlorobenzene
  • 1,4-Dichlorobenzene
  • 1,4-Dichlorobutane
  • 2-Chloroethylvinylether
  • Benzene
  • Bromodichloromethane
  • Bromoform
  • Bromomethane
  • Carbon tetrachloride
  • Chlorobenzene
  • Chloroethane
  • Chloroform
  • Chloromethane
  • cis-1,3-Dichloropropene
  • Dibromochloromethane
  • Ethylbenzene
  • Methylene chloride
  • Tetrachloroethylene
  • Toluene
  • trans-1,2-Dichloroethene
  • trans-1,3-Dichloropropene
  • Trichloroethylene
  • Trichlorofluoromethane
  • Vinyl chloride

Materials

     
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