US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms, Fast GC Analysis

US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms, Fast GC Analysis

Conditions

column SLB-5ms, 20 m x 0.18 mm I.D., 0.18 µm (28564-U)
oven 45 °C, 86 C/min to 130 °C (1.73 min), 20 °C/min to 180 °C, 12 °C/min to 240 °C, 20 °C/min to 330 °C (2 min)
carrier gas helium, 1.4 mL/min, constant
sample 109 component semivolatile standard (each analyte at 2 ppm), plus 3 surrogate and 3 internal standard compounds (each at 5 ppm) in ethyl acetate
injection 1 µL splitless (0.75 min)
liner 2 mm I.D. fast FocusLiner™ liner with taper
inj. temp. 275 °C
MSD interface 330 °C
scan range m/z = 40-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Food and Beverages
Legal Information FocusLiner is a trademark of SGE Analytical Science Pty Ltd., SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,1-Dichloro-2,2-bis(4-chlorophenyl)ethane (4,4′-DDD)
  • 1,3-Dimethyl-2-nitrobenzene
  • 2,2′,3,3′,4,4′,6-Heptachlorobiphenyl
  • 2,2′,3,3′,4,5′,6,6′-Octachlorobiphenyl
  • 2,2′,3′,4,6-Pentachlorobiphenyl
  • 2,2′,4,4′,5,6′-Hexachlorobiphenyl
  • 2,2′,4,4′-Tetrachlorobiphenyl
  • 2,3-Dichlorobiphenyl
  • 2,4′,5-Trichlorobiphenyl
  • 2,4-Dinitrotoluene
  • 2,6-Dinitrotoluene
  • 2-Butanol
  • 2-Chlorobiphenyl
  • 4,4′-DDE (1,1-Dichloro-2,2-bis(p-chlorophenyl)ethylene)
  • 4,4′-DDT
  • Acenaphthene-d10
  • Acenaphthylene
  • Alachlor
  • Aldrin
  • Ametryn
  • Anthracene
  • Atraton
  • Atrazine
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Benzylbutylphthalate
  • Bis(2-ethylhexyl) adipate
  • Bis(2-ethylhexyl) phthalate
  • Bromacil
  • Butachlor
  • Carboxine
  • Chlorobenzilate
  • Chloroneb
  • Chlorothalonil
  • Chlorpropham
  • Chlorpyrifos
  • Chlorthal-dimethyl
  • Chrysene
  • Chrysene-d12
  • cis-Permethrin
  • Cyanazine
  • Cycloate
  • Diazinon
  • Dibenzo[a,h]anthracene
  • Dibutyl phthalate
  • Dichlorvos
  • Dieldrin
  • Diethyl phthalate
  • Dimethylphthalate
  • Diphenamid
  • Disulfoton
  • Endosulfan sulfate
  • Endrin
  • Endrin aldehyde
  • Endrin ketone
  • Ethoprophos
  • Etridiazole
  • Fenamiphos
  • Fenarimol
  • Fluorene
  • Fluridon
  • Heptachlor
  • Heptachlor exo-epoxide
  • Hexachlorobenzene
  • Hexachlorocyclopentadiene
  • Hexazinone
  • Indeno[1,2,3-cd]pyrene
  • Isophorone
  • Lindane
  • Merphos
  • Methoxychlor
  • Metolachlor
  • Metribuzin
  • Mevinphos
  • Molinate
  • N-(2-Ethylhexyl)-5-Norbornene-2,3-Dicarboximide
  • N,N-Diethyl-2-(1-naphthyloxy)propanamide
  • Norflurazon
  • Paraoxon-methyl
  • Pebulat
  • Pentachlorophenol
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d10
  • Prometon
  • Prometryn
  • Propachlor
  • Propazine
  • Propyzamide
  • Pyrene
  • S-Ethyl-N,N-dipropylthiocarbamate
  • Simazine
  • Simetryn
  • Tebuthiuron
  • Terbacil
  • Terbufos
  • Terbutryn
  • Tetrachlorvinphos
  • trans-Nonachlor
  • trans-Permethrin
  • Triadimefon
  • Tricyclazone
  • Trifluralin
  • Triphenyl phosphate
  • Vernolat
  • α-1,2,3,4,5,6-Hexachlorocyclohexane
  • α-Chlordane
  • α-Endosulfan
  • β-BHC
  • β-Endosulfan
  • γ-Chlordane
  • δ-BHC

Materials

     
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