US EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on SLB®-5ms (30 m x 0.25 mm I.D., 0.50 μm)

US EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on SLB®-5ms (30 m x 0.25 mm I.D., 0.50 μm)

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.50 µm (28473-U)
oven 40 C (1 min), 12 C/min to 250 C, 25 C/min to 340 C (4.5 min)
carrier gas helium, 1.5 ml/min constant
sample 50 ng on-column of a 62 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column)
injection 1.0 µL, splitless (0.50 min)
liner 4 mm I.D., single taper
inj. temp. 250 C
MSD interface 340 C
scan range m/z = 40-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,2,4,5-Tetrachlorobenzene
  • 1,2-Dichlorobenzene-d4
  • 1,3,5-Trinitrobenzene
  • 1,3-Dinitrobenzene
  • 1,4-Dichlorobenzene-d4
  • 1,4-Dinitrobenzene
  • 1,4-Dioxane
  • 1,4-Naphthoquinone
  • 1-Methylnaphthalene
  • 1-Naphthylamine
  • 2,3,4,6-Tetrachlorophenol
  • 2,3,5,6-Tetrachlorophenol
  • 2,4,6-Tribromophenol
  • 2,6-Dichlorophenol
  • 2-Acetylaminofluorene
  • 2-Chlorophenol-d4
  • 2-Fluorobiphenyl
  • 2-Fluorophenol
  • 2-Naphthylamine
  • 2-Picoline
  • 3-Methylcholanthrene
  • 3-Methylphenol
  • 4-Aminobiphenyl
  • 4-Dimethylaminoazobenzene
  • 4-Nitroquinoline-1-oxide
  • 5-Nitro-o-toluidine
  • 7,12-Dimethylbenz[a]anthracene
  • Acenaphthene-d10
  • Acetophenone
  • Aniline
  • Benzyl alcohol
  • Chlorobenzilate
  • Chrysene-d12
  • Diallate isomer
  • Dibenzo[a,j]acridine
  • Dimethoate
  • Dinoseb
  • Diphenylamine
  • Disulfoton
  • Ethyl methanesulfonate
  • Famphur
  • Hexachloropropene
  • Isodrin
  • Isosafrole isomer
  • Methapryilene
  • Methyl methanesulfonate
  • Methyl parathion
  • Naphthalene-d8
  • Nitrobenzene-d5
  • N-Nitrosodiethylamine
  • N-Nitroso-di-n-butylamine
  • N-Nitrosomethylethylamine
  • N-Nitrosomorpholine
  • N-Nitrosopiperidine
  • N-Nitrosopyrrolidine
  • o,o,o-Triethyl phosphorothioate
  • o-Toluidine
  • Parathion
  • Pentachlorobenzene
  • Pentachloroethane
  • Pentachloronitrobenzene
  • Perylene-d12
  • Phenacetin
  • Phenanthrene-d10
  • Phenol-d6
  • Phorate
  • p-Phenylenediamine
  • Pronamide
  • p-Terphenyl-d14
  • Pyridine
  • Safrole
  • Sulfotep
  • Thionazin
  • α,α-Dimethylphenethylamine

Materials

     
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