US EPA Method 8270: GC Analysis of Semivolatiles on SLB-5ms (20 m x 0.18 mm I.D., 0.36 μm), Fast GC Analysis

US EPA Method 8270: GC Analysis of Semivolatiles on SLB-5ms (20 m x 0.18 mm I.D., 0.36 μm), Fast GC Analysis

Conditions

column SLB-5ms, 20 m x 0.18 mm I.D., 0.36 µm (28576-U)
oven 40 °C (1 min), 12 °C/min to 200 °C, 20 °C/min to 340 °C (2 min)
carrier gas helium, programmed flow; 0.5 mL/min (5 min hold), to 1 mL/min at 5.5 min (constant for remainder of run)
sample 80 °Component semivolatile standard at 50 ppm plus 6 internal standards (at 40 ppm) in methylene chloride
injection 0.50 µL, pulsed splitless (25 psi until 0.1 min) (0.75 min)
liner 4 mm I.D., single taper
inj. temp. 250 °C
MSD interface 340 °C
scan range m/z 40-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,2,4-Trichlorobenzene
  • 1,2-Dichlorobenzene
  • 1,2-Dichlorobenzene-d4
  • 1,3-Dichlorobenzene
  • 1,4-Dichlorobenzene
  • 1,4-Dichlorobenzene-d4
  • 2,4,5-Trichlorophenol
  • 2,4,6-Tribromophenol
  • 2,4,6-Trichlorophenol
  • 2,4-Dichlorophenol
  • 2,4-Dimethylphenol
  • 2,4-Dinitrophenol
  • 2,4-Dinitrotoluene
  • 2,6-Dinitrotoluene
  • 2-Chloronaphthalene
  • 2-Chlorophenol
  • 2-Chlorophenol-d4
  • 2-Fluorobiphenyl
  • 2-Fluorophenol
  • 2-Methyl-4,6-dinitrophenol
  • 2-Methylnaphthalene
  • 2-Methylphenol
  • 2-Nitroaniline
  • 2-Nitrophenol
  • 3,3′-Dichlorobenzidine
  • 3,3′-Dimethylbenzidine
  • 3-Nitroaniline
  • 4-Bromophenylphenylether
  • 4-Chloro-3-methylphenol
  • 4-Chloroaniline
  • 4-Chlorophenylphenyl ether
  • 4-Methylphenol
  • 4-Nitroaniline
  • 4-Nitrophenol
  • Acenaphthene
  • Acenaphthene-d10
  • Acenaphthylene
  • Aniline
  • Anthracene
  • Azobenzene
  • Benzidine
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Benzoic acid
  • Benzyl alcohol
  • Bis(2-chloroethoxymethane)
  • Bis(2-chloroethyl) ether
  • Bis(2-chloroisopropyl) ether
  • Bis(2-ethylhexyl) phthalate
  • Butylbenzylphthalate
  • Carbazole
  • Chrysene
  • Chrysene-d12
  • Dibenzo[a,h]anthracene
  • Dibenzofuran
  • Diethyl phthalate
  • Dimethylphthalate
  • Di-n-Butyl phthalate
  • Di-n-Octyl phthalate
  • Fluoranthene
  • Fluorene
  • Hexachlorobenzene
  • Hexachlorobutadiene
  • Hexachlorocyclopentadiene
  • Hexachloroethane
  • Indeno[1,2,3-cd]pyrene
  • Isophorone
  • Naphthalene
  • Naphthalene-d8
  • Nitrobenzene
  • Nitrobenzene-d5
  • N-Nitrosodimethylamine
  • N-Nitroso-di-n-propylamine
  • N-Nitrosodiphenylamine
  • Pentachlorophenol
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d12
  • Phenol
  • Phenol-d6
  • Pyrene
  • Pyridine
  • Terphenyl-d12

Materials

     
Related Links