US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms

US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 60 °C (1 min), 10 °C/min to 340 °C (5 min)
carrier gas helium, 1.5 mL/min. constant
sample 22 component TO-13 standard plus 5 internal standards at 500 ppb in hexane:ethyl ether (90:10)
injection 1.5 µL, pulsed (25 psi until 0.2 min) splitless (0.75 min)
liner 2 mm I.D. FocusLiner™ liner (2879601-U)
inj. temp. 250 °C
MSD interface 330 °C300 °C / 200 °C (source/quads)
scan range m/z 40-450

Description

Categories Analytical Chromatography, GC Applications, PAHs, Hydrocarbons, Semivolatiles
Featured Industry Environmental
Industrial Hygiene
Legal Information FocusLiner is a trademark of SGE Analytical Science Pty Ltd., SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,4-Dichlorobenzene-d4
  • Acenaphthene
  • Acenaphthene-d10
  • Acenaphthylene
  • Anthracene
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[e]pyrene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Chrysene
  • Chrysene-d12
  • Coronene
  • Dibenzo[a,h]anthracene
  • Fluoranthene
  • Fluorene
  • Fluorene-d10
  • Indeno[1,2,3-cd]pyrene
  • Naphthalene
  • Naphthalene-d8
  • Perylene
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d10
  • Pyrene
  • Pyrene-d10

Materials

     
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