HPLC Analysis of cis/trans-Dothiepin Enantiomers on Astec® CYCLOBOND® I 2000 AC

HPLC Analysis of cis/trans-Dothiepin Enantiomers on Astec® CYCLOBOND® I 2000 AC

Conditions

column CYCLOBOND I 2000 AC, 25 cm x 4.6 mm I.D., 5 µm particles (20124AST)
column temp. 22 C
mobile phase [A] 1.0% triethylamine acetate, pH 4.1; [B] acetonitrile; (85:15, A:B)
flow rate 1 ml/min
sample 1 mg/mL in methanolpeak 1: 9.48 min.peak 2: 12.48 min.
injection 2 µl
detector UV, 254 nm

Description

Categories Analytical Chromatography, Chiral Applications, Antidepressants, Pharmaceutical (small molecule), All Pharmaceutical Applications
Featured Industry Pharmaceutical (small molecule)
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CYCLOBOND is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for HPLC

Materials

     
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