LC/MS Analysis of Antifungals on Ascentis® Express Biphenyl

LC/MS Analysis of Antifungals on Ascentis® Express Biphenyl

Conditions

column Ascentis Express Biphenyl, 10 cm x 2.1 mm I.D., 2.7 µm particles (64065-U)
column temp. 35 °C
mobile phase [A] 10 mM ammonium acetate; [B] acetonitrile
gradient 2% B for 1 min; to 100% B in 10 min; held at 100% B for 1 min
flow rate 0.3 mL/min
pressure 2925 psi (201 bar)
sample Antifungals, 1-10 µg/mL in 99:1, water:methanol
injection 0.5 µL
detector MS, ESI+, XIC

Description

Categories Analytical Chromatography, Antifungals
Featured Industry Pharmaceutical (small molecule)
Legal Information Ascentis is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for LC-MS

Materials

     
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