LC/MS Analysis of Fluoroamphetamine Drugs of Abuse on Ascentis® Express HILIC

LC/MS Analysis of Fluoroamphetamine Drugs of Abuse on Ascentis® Express HILIC

Conditions

column Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 µm particles (53939-U)
column temp. 35 °C
gradient 5 mM ammonium formate in acetonitrile:water (90:10, v/v)
flow rate 0.4 mL/min
sample 300 ng/mL in acetonitrile
injection 2 µL
detector TOF/MS

Description

Analysis Note The fluoroamphetamines (FA) are a group of "designer" stiµLant drugs in amphetamine family. The rapid LC/MS analysis of four members of the FA family on Ascentis Express HILIC is shown here. Cerilliant CRMs were used to ensure reliable MS identification and quantification.
Categories Analytical Chromatography, Forensics and Toxicology, drugs of abuse, Drugs of Abuse
Featured Industry Forensics and Toxicology
Legal Information Ascentis is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for HPLC

Materials

     
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