UHPLC Analysis of Flakka and Related Compounds on Titan™ Silica in HILIC Mode

UHPLC Analysis of Flakka and Related Compounds on Titan™ Silica in HILIC Mode

Conditions

column Titan Silica, 10 cm x 2.1 mm I.D., 2 µm (581532-U)
column temp. 35 °C
mobile phase 10 mM ammonium formate in acetonitrile:water (95:5)
flow rate 0.4 mL/min
sample 50 µg/mL in methanol:acetonitrile (10:90)
injection 1 µL
detector UV, 265 nm

Description

Analysis Note The rapid separation of the street drug Flakka (α-PVP) and related compounds is shown here on a Titan Silica column in HILIC mode. Highest grade UHPLC solvents were used to supply low background interference and low particulate contamination for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
Categories Analytical Chromatography, Drugs of Abuse
Featured Industry Forensics and Toxicology
Legal Information Titan is a trademark of Sigma-Aldrich Co. LLC
suitability suitable for HPLC

Materials

     
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