Analytical Method: Boron in silicon tetrachloride

Instruments and Reagents:

Cat.No. 173016  Spectroquant®VIS Spectrophotometer Prove 100 or

Cat.No. 173017  Spectroquant® UV/VIS Spectrophotometer Prove 300 or

Cat.No. 173018  Spectroquant® UV/VIS Spectrophotometer Prove 600 or

Cat.No. 109748  Spectroquant® Phometer NOVA 30 or

Cat.No. 109751  Spectroquant® Photometer NOVA 60

Cat.No. 114946  Rectangular cells 10 mm and/or

Cat.No. 114947  Rectangular cells 20 mm and/or

Cat.No. 114944  Rectangular cells 50 mm
Cat.No. 114839  Spectroquant® Boron Test
Cat.No. 106498  Sodium hydroxide for analysis
Cat.No. 116754  Water for analysis
 
Sodium hydroxide solution:
Dissolve 1.2 g sodium hydroxide for analysis in 50 ml of water for analysis.
 
Sample preparation:
Dissolve 1.2 g of sodium hydroxide in 50 ml water for analysis. Use a Plastic - syringe with hollow needle to measure out 0.6 ml of SiCl4. Pure it into the previously prepared NaOH-solution. Determine the weight of the SiCl4 by differential weighing. Heat the mixture in order to dissolve any precipitated silicon acid and transfer to a 100-ml volumetric flask, fill up to volume with water for analysis and mix well.
 
Analysis:
Determine with the above mentioned test kit.
 
Calculation:

Boron content in %  =   analysis value in mg/l B x 10
weight of sample in mg

 

 

 

Materials

     
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