Analytical Method: Copper (total) in cyanidic plating baths

Instruments and Reagents:

Cat.No. 173016  Spectroquant® VIS Spectrophotometer Prove 100 or

Cat.No. 173017  Spectroquant® UV/VIS Spectrophotometer Prove 300 or

Cat.No. 173018  Spectroquant® UV/VIS Spectrophotometer Prove 600 or

Cat.No. 109748  Spectroquant® Photometer NOVA 30 or

Cat.No. 109751  Spectroquant® Photometer NOVA 60 or

Cat.No. 173632  Spectroquant® Colorimeter Move 100

Cat.No. 114946  Rectangular cells 10 mm and/or

Cat.No. 114947  Rectangular cells 20 mm and/or

Cat.No. 114944  Rectangular cells 50 mm
Cat.No. 114553  Spectroquant® Copper Cell Test
Cat.No. 114767  Spectroquant® Copper Test
Cat.No. 107209  Hydrogen peroxide 30 % (Perhydrol®) for analysis
Cat.No. 116754  Water for analysis
 
Sample preparation:
Place 5 ml of the bath solution in a 500-ml volumetric flask and fill up to volume with water for analysis. Take
5 ml from this solution and fill up to 500 ml, with water for analysis, to give a 1:10000 dilution.
Pipet 10 ml of this final dilution into a test-tube, add 1 drop of Perhydrol®, mix and allow to stand for 1 minute. The further treatment is as given in the manual.
 
Analysis:
Determine with the above mentioned test kits
 
Calculation:
Copper (total) content in g/l Cu = analysis value in mg/l Cu x 10

Materials

     
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