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Analysis of Vitamin D in Milk and Infant Formula using UHPLC/MS/MS per AOAC Method 2011.11
While quantitative analysis was performed for Vitamins D2 and D3, the samples were scanned for the presence of the 25-hydroxy metabolites.
Analysis of Residual Solvents in Hemp Extract by Headspace SPME-GC/MS
The use of solid phase microextraction (SPME) allowed for the straightforward, fast, sensitive, and accurate GC/MS determination of the residual solvent content of spiked and unspiked samples of hemp extract.
Food & Beverage Analysis: Sugars & Saccharides
Simple sugars using hydrophilic interaction chromatography (HILIC): Chromatographic analysis of simple sugars can be challenging because these compounds are highly polar, uncharged, and lack a chromophore. The preferred mode of HPLC separation is HILIC because it provides the advantage of...
Increase Removal of Fat and Pigment from Avocado Extracts Prior to GC-MS Analysis of Pesticide and Metabolite Residues
Supelco's Z-Sep+ sorbent effectively removes fat and pigment interferences from avocado, with good pesticide recoveries; it removes more matrix than traditional PSA/C18 sorbent, and produces a lower background for GC-MS analysis.
GC Analysis of Fatty Acids in Walnuts and Peanuts
Determination of the fatty acid composition of nuts using established methods for GC analysis on capillary columns of 3 selectivities: Omegawax, SP-2560, and ionic liquid based SLB-IL111.
Fast Extraction and Low Level Detection of Chloramphenicol in Shrimp
A highly selective and sensitive analytical method was developed for chloramphenicol using a QuEChERS type sample preparation approach and LC-MS/MS detection.
Enzymatic Method for Determining D-Sorbitol (D-Sorbitol Assay)
Assay protocol for the colorimetric detection of D-Sorbitol in samples using the D-Sorbitol assay kit.
Analytical Method: Phosphorus (Total) in Dairy Products
Phosphorus (total) in dairy products - Photometric determination using the Phosphorus molybdenum blue method subsequent to acid mineralisation
Derivatization of Fatty acids to FAMEs
Explore how GC can be used to analyze fatty acids either as free fatty acids or as fatty acid methyl esters.
Zinc (Total) in Beer Worts
Photometric determination subsequent to acid mineralisation with sulfuric acid and Perhydrol;
Determination of Fatty Acid Content in Infant Formula by GC/FID Using the SP-2560 Capillary Column per AOAC Method 2012.13
AOAC method 2012.13 was applied to the analysis of powdered infant formula for the identification and quantitation of all labeled fatty acids and fatty acid groups.
Development of a Method for Analysis of Phthalate Esters in Vegetable Oils
Rapid, easy, sensitive method for the anaysis of PAEs, using LLE and direct immersion SPME, demonstrated good accuracy, repeatability, linearity and LOQ.
Analytical Method for Determination of the Solution Color of Raw Sugars, Brown Sugars and Colored Syrups at pH 7.0 (According to ICUMSA Method GS1/3-7)
Method: Spectrophotometric Color Determination at 420 nm Zero adjustment For each measurement series, a zero adjustment is required. It is recommended to use the same cell for zero adjustment and for sample measurement. The zeroing procedure for the measurement series is automatically prompted by...
Enzymatic Food Analysis
Enzymatic methods for food analysis are highly specific and offer considerable time and cost savings over other methods, especially from the sample preparation standpoint. We offer a wide variety of convenient kits and reagents for rapid and reliable enzymatic food...
Enzymatic Method for Determining Galactose (Galactose Assay)
This assay protocol is suitable for the colorimetric/fluorometric detection of Galactose and Lactose in cell and tissue culture supernatants, urine, plasma, serum, and other biological samples using the Galactose Assay Kit.
Enzymatic Galactose and Lactose Assay Protocol
This assay protocol is suitable for the colorimetric/fluorometric detection of Galactose and Lactose in cell and tissue culture supernatants, urine, plasma, serum, and other biological samples using the Galactose and Lactose Assay Kit (MAK011). In this assay kit, galactose is...
Testing Food for Fipronil Contamination
Test your food for fipronil contamination using our analytical standards, certified reference materials, solvents, and columns for analysis.
Veterinary Drug Residues
The use of veterinary drugs may be integral to the process of raising food producing animals and fish. These can include antibiotics, hormones, and steroids.
Improved Determination of Volatile Organic Compounds in Water by SPME and GC/MS: ISO Standard 17944
High performance, reliability, and reproducibility of HS-SPME in combination with GC/MS for the determination of VOCs in water was proven in an interlaboratory trial. The new ISO 17943 using HS-SPME is an improvement on existing official methods for this determination...
Determination of Bisphenol A in Drinking Water
A comprehensive sample preparation and analytical procedure was developed by Supelco for determining BPA in drinking water.
Aminoglycoside Analysis in Pork Muscle using Molecularly Imprinted Polymer Cleanup and LC/MS/MS Detection
Extraction and quantitative analysis of aminoglycosides in porcine tissue, using molecular imprinted polymer solid phase extraction followed by LC-MS/MS.
Trans Fats in Cookies using SP-2560 and SLB-IL111
Extraction of lipids as fatty acids, and subsequent detection of trans fats from a cookie sample made using partially hydrogenated vegetable oils - a Supelco technical article
Cannabis Terpene Analysis by Headspace SPME GC/MS
High-resolution profiling of terpenes and terpenoids to identify fragrance compounds and distinguish hops and cannabis varieties using SPME-GC/MS.
Measuring Peroxidase in Milk
Application Note: Peroxidase in milk – Visual determination after conversion of a specific substrate
Determination of Additives in Beverages Using Ascentis® Express Columns
RP-Amide and HILIC, both amenable to the analysis of polar compounds, were successfully used to resolve several beverage components, including sugars, vitamins, sweeteners, preservatives, and caffeine.
Analysis of Polychlorinated Biphenyls in Fish Oil Using Supelclean™ EZ-POP NP, Silica Gel SPE, and an SLB®-5ms GC Column
Polychlorinated biphenyls (PCBs) were once widely used in many industrial and commercial applications such as insulating fluids, dielectrics, and lubricants. This included their extensive use in electrical transformers. PCB use has been banned in many countries, and the Stockholm Convention...
Analysis of Aflatoxin B1, B2, G1, and G2 in Corn Meal, Wheat Meal, and Raw Peanut Paste Matrices
Supel™ Tox AflaZea SPE cartridges provide exceptional cleanup of corn meal, wheat meal, and raw peanut paste, yielding high analyte recoveries and low %RSD for aflatoxin analysis.
Quantifying Picogram Concentrations of Aflatoxin M1 in Liquid Milk Using SPE Cleanup and LC/MS Analysis
Fast method for the cleanup, analysis, and quantification of aflatoxin M1 in milk samples to EU regulatory standards (0.025 μg/kg).
Analytical Method: Nitrite in potato instant powder
Photometric determination using the Griess method subsequent to extraction
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