KITALYSISBASE

KitAlysis^™ High-Throughput Base Screening Kit - Pack of 2

• Sinônimo(s): Base screen, Base screening kit, KitAlysis base
• NACRES: NA.22
• UNSPSC Code: 12161600

Propriedades

• product line: KitAlysis^™
• reaction suitability: reaction type: Buchwald-Hartwig Cross Coupling Reaction, reaction type: Cross Couplings, reaction type: Heck Reaction, reaction type: Hiyama Coupling, reaction type: Negishi Coupling, reaction type: Sonogashira Coupling, reaction type: Stille Coupling, reaction type: Suzuki-Miyaura Coupling
• functional group: phosphine

Descrição

Application

Versatile base screening kit for cross-coupling reactions and other synthetic transformations. Step-by-step user guide and a downloadable experimental excel sheet are provided in the below hyperlinks.

Step-by-Step Guide for KitAlysis High-Throughput Base Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that contain the following:

• 7 X 2 pre-weighed bases (30 μmol) in individual microvials with magnetic stir bars
• 4 X 2 base solutions
• 2 empty microvials for Chemist′s Choice of base allowing customization
• 4 degassed anhydrous solvents (DMF, MeOH, THF, Toluene)
• 2 NEW KitAlysis 24-Well Reaction Block Replacement Films
• 4 empty substrate stock solution reaction vials with stirbars

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

• Designed and tested by synthetic chemists
• Easily run 24-microscale reactions in parallel
• 10 μmol reactions with 3 equiv. base, 0.1 M concentration
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Somente componentes do kit

• Potassium bicarbonate, ACS reagent, 99.7%, powder, crystals or granules

Componentes do kit também disponíveis separadamente

• RDD019

  Potassium phosphate tribasic, anhydrous, free-flowing, Redi-Dri^™, reagent grade, ≥97%

  SDS
• 441902

  Cesium carbonate, ReagentPlus^®, 99%

  SDS
• 757551

  Potassium hydroxide, ≥99.95% trace metals basis

  SDS
• 791733

  Potassium acetate, anhydrous, free-flowing, Redi-Dri^™, ACS reagent, ≥99.0%

  SDS
• 139009

  1,8-Diazabicyclo[5.4.0]undec-7-ene, 98%

  SDS
• 225770

  Lithium bis(trimethylsilyl)amide solution, 1.0 M in THF

  SDS
• 702706

  Sodium tert-butoxide solution, 2 M in THF, ZerO₂^®

  SDS

Ver tudo (16)

Informações de segurança

• pictograms: GHS02,GHS06,GHS08,GHS05
• signalword: Danger
• hcodes: H225,H251,H301 + H311 + H331,H304,H314,H335,H336,H351,H360D,H370,H373,H412
• Classe de armazenamento: 4.1B - Flammable solid hazardous materials
• flash_point_f: -5.8 °F
• flash_point_c: -21 °C
• wgk: WGK 2
• pcodes: P210 - P280 - P301 + P330 + P331 - P303 + P361 + P353 - P304 + P340 + P310 - P305 + P351 + P338
• Hazard Classifications: Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Chronic 3 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Self-heat. 1 - Skin Corr. 1A - STOT RE 2 Inhalation - STOT SE 1 - STOT SE 3
• target_organs: Central nervous system, Eyes,Central nervous system, Respiratory system
• supp_hazards: EUH014,EUH019