If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdf
650463
Diclorometano
HPLC Plus, for HPLC, GC, and residue analysis, ≥99.9%, contains 50-150 ppm amylene as stabilizer
Sinônimo(s):
cloreto de metileno, Cloreto de metileno
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Sobre este item
gas chromatography (GC): suitable
6.83 psi ( 20 °C)
Pular para
Nome do produto
Diclorometano, HPLC Plus, for HPLC, GC, and residue analysis, ≥99.9%, contains 50-150 ppm amylene as stabilizer
InChI key
YMWUJEATGCHHMB-UHFFFAOYSA-N
InChI
1S/CH2Cl2/c2-1-3/h1H2
SMILES string
ClCCl
grade
HPLC Plus
vapor density
2.9 (vs air)
vapor pressure
24.45 psi ( 55 °C)
6.83 psi ( 20 °C)
assay
≥99.9%
form
liquid
autoignition temp.
1223 °F
contains
50-150 ppm amylene as stabilizer
expl. lim.
22 %
technique(s)
HPLC: suitable
gas chromatography (GC): suitable
impurities
≤ 1.0 ppb Fluorescence (quinine) at 365 nm
≤0.01% water
evapn. residue
≤0.0001%
halogenated residue
≤10 ng/L (as heptachlor epoxide)
refractive index
n20/D 1.424 (lit.)
bp
39.8-40 °C (lit.)
mp
−95 °C (lit.)
density
1.325 g/mL at 25 °C (lit.)
λ
H2O reference
UV absorption
λ: 235 nm Amax: 1.0
λ: 240 nm Amax: 0.10
λ: 250 nm Amax: 0.02
λ: 300-400 nm Amax: 0.005
suitability
suitable for residue analysis
Quality Level
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1 of 4
Este Item | 1.06044 | 676853 | 320269 |
|---|---|---|---|
| grade HPLC Plus, for residue analysis | grade - | grade ACS reagent | grade ACS reagent |
| Quality Level 100 | Quality Level 100 | Quality Level 200 | Quality Level 200 |
| assay ≥99.9% | assay ≥99.9% (GC) | assay ≥99.5% | assay ≥99.5% |
| technique(s) HPLC: suitable, gas chromatography (GC): suitable | technique(s) HPLC: suitable | technique(s) - | technique(s) - |
| form liquid | form liquid | form liquid | form liquid |
| vapor pressure 24.45 psi ( 55 °C), 6.83 psi ( 20 °C) | vapor pressure 24.45 psi ( 55 °C), 6.83 psi ( 20 °C) | vapor pressure 24.45 psi ( 55 °C), 6.83 psi ( 20 °C) | vapor pressure 24.45 psi ( 55 °C), 6.83 psi ( 20 °C) |
Application
- Extração de neonicotinoides de amostras de mel junto com acetonitrila usando microextração líquido-líquido dispersiva (DLLME)
- Extração com solvente ultrassônico e limpeza de amostras de café torrado para a análise de 7 resíduos de pesticidas por cromatografia líquida-espectrometria de massa em tandem (LC-MS/MS)
- Pré-concentração adicional baseada em DLLME dos extratos de amostra na análise de três anfenicóis em produtos alimentícios de origem animal por HPLC com detecção de UV
- Remoção da fase orgânica dos extratos de amostra de solo obtidos na determinação de dois herbicidas de sulfonilureia usando HPLC
- Teste de quatro solventes de extração no desenvolvimento de um método baseado em detecção amperométrica por HPLC para a análise de três resíduos de carbamato em amostras de alimentos líquidos e sólidos
- Extração de metrafenona de amostras de vegetais por dispersão de matriz em fase sólida (método MSPD) seguida de análise por HPLC
Other Notes
Packaging
Como líder global em reagentes de laboratório, estamos sempre à procura de novas formas de otimizar a segurança dos nossos produtos. O design recém-desenvolvido do frasco de solvente de 4L apresenta tecnologia de vedação avançada que elimina vazamentos para tornar o manuseio de solventes mais seguro e mais conveniente do que nunca.
Veja todos os novos recursos aqui!
Legal Information
signalword
Warning
hcodes
Hazard Classifications
Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Central nervous system
Classe de armazenamento
6.1D - Non-combustible acute toxic Cat.3 / toxic hazardous materials or hazardous materials causing chronic effects
wgk
WGK 2
flash_point_f
does not flash
flash_point_c
does not flash
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Artigos
Highly accurate HPLC-FLD method for evaluating 15 PAHs in olive oil using Ascentis® Express PAH HPLC column and SPE cleanup, following GB 5009.265-2021.
Nitrosamines analysis by solid phase extraction (SPE) and subsequent gas chromatography-tandem mass spectrometry (GC-MS/MS) according to GB 5750.10-2023.
Protocolos
In the present study we demonstrate compliance of silica gel 60 F254 HPTLC plates with USP requirements, and how HPTLC plates are suitable for the Sildenafil citrate-Limit of Imidazole test.
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The 4L M-Bottle provides safe handling of solvents due to an innovative solvent bottle design with sealing technology to eliminate leaks and reduce risks in solvent dispensing.
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How is shipping temperature determined? And how is it related to the product storage temperature?
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Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf
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