KITALYSIS-SM

KitAlysis^™ High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4

• Synonym(s): Suzuki-Miyaura Cross-Coupling
• NACRES: NA.22
• UNSPSC Code: 12161600

Properties

• product line: KitAlysis^™
• reaction suitability: reaction type: Cross Couplings, reaction type: Suzuki-Miyaura Coupling, reagent type: catalyst; core: palladium
• functional group: phosphine

Description

Application

Screening kit for Suzuki-Miyaura cross-coupling reaction. Step-by-step user guide and a downloadable experimental excel sheets are provided in the below hyperlink.
Step-by-Step Guide for Suzuki-Miyaura Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet

Each kit contains 4 customizable screening sets that include the following components:

• 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
• 1 (2 mL) ampule each of Toluene, THF, n-Butanol, DMAc, and aq. 1.5 M K₃PO_4.
• 4 NEW KitAlysis 24-Well Reaction Block Replacement Films.
• 4 substrate reaction vials with stir bars.
• 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reactions in parallel.
• 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit Components Only

• SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

Kit Components Also Available Separately

• 732117

  Pd-PEPPSI^™-IPent catalyst, ≥95% 5 µmol

  SDS
• 753009

  SPhos Pd G2 5 µmol

  SDS
• 761311

  cataCXium^® A Pd G2 5 µmol

  SDS
• 763381

  XPhos Pd G3, 98%, 1:1 MTBE adduct 5 µmol

  SDS
• 764175

  P(Cy₃) Pd G3, 97% 5 µmol

  SDS
• 764183

  APhos Pd G3, 97% 5 µmol

  SDS
• 900522

  Toluene, anhydrous, ZerO₂^®, 99.8% 8 mL

  SDS

See All (12)

Safety Information

• pictograms: GHS02,GHS08,GHS05,GHS07,GHS09
• signalword: Danger
• hcodes: H225,H302 + H312 + H332,H304,H315,H318,H335,H336,H351,H360D,H373,H410
• pcodes: P210 - P273 - P280 - P301 + P310 - P305 + P351 + P338 - P331
• target_organs: Central nervous system, Respiratory system
• supp_hazards: EUH019
• Storage Class: 3 - Flammable liquids
• flash_point_f: 1.4 °F
• flash_point_c: -17 °C
• wgk: WGK 3
• Hazard Classifications: Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3