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1.88052

Supelco

Water standard 1%

Certified Reference Material for volumetric Karl Fischer Titration 1 g ≙ 10 mg H₂O Aquastar®

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grade

certified reference material

Quality Level

Agency

ISO (17025, 17034)

product line

Aquastar®

form

liquid

autoignition temp.

287 °C (DIN 51794,Information refers to the main component.)

expl. lim.

1.7 % (v/v)

technique(s)

Karl-Fischer titration: suitable
titration: suitable

bp

119 °C/1013 hPa

mp

-95 °C

transition temp

flash point 31 °C (Information refers to the main component.)

density

0.92 g/cm3 at 20 °C

format

single component solution

storage temp.

15-25°C

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format

single component solution

format

single component solution

format

neat

grade

certified reference material

grade

certified reference material

grade

reference material

grade

certified reference material

product line

Aquastar®

product line

Aquastar®

product line

Aquastar®

product line

Aquastar®

form

liquid

form

liquid

form

liquid

form

solid

autoignition temp.

287 °C (DIN 51794,Information refers to the main component.)

autoignition temp.

287 °C (Information refers to the main component.)

autoignition temp.

465 °C

autoignition temp.

-

General description

Water standard 1% is prepared using high-purity water and reagents by the gravimetric method. Its characterization is carried out at an accredited quality control (QC) laboratory according to DIN EN ISO/IEC 17025. The water content of the standard is measured by direct coulometric Karl Fischer titration, in accordance with ISO 760.

Please visit ISO certificates and Site Quality Self-Assessments to access the current certificates of accreditation.

Download your certificate at http://www.sigma-aldrich.com to view certified values, including uncertainty and expiry date.

Application

Water standard 1% can be used for:
  • Evaluating the accuracy of coulometric Karl Fischer titrators according to ISO 9001 chapter 7.1.5 “Monitoring and measuring resources” as a Certified reference material (CRM)
  • Checking the accuracy of measured results according to European Pharmacopeia (Ph.Eur.) chapter 2.5.32 “Water Micro Determination”
  • Standardizing titrants according to European Pharmacopeia (Ph.Eur.) chapter 2.5.12 “Water Semi-Micro Determination” and the United States Pharmacopeia <921> “Water Determination”
  • Titer determinations using volumetric method with one component and two component reagents

Features and Benefits

  • Packed in convenient 8 mL glass ampoules and 10 single-use ampoules in a box
  • Supplied with a batch-specific certificate of analysis (CoA) having data on the exact measured water content of the batch, uncertainty, method of analysis, the NIST batch, and minimum shelf life
  • Measured and qualified in an ISO/IEC 17025 and ISO 17034 accredited calibration laboratory
  • Directly traceable to SI unit (kg) and verified by SRM 2890 from NIST

Packaging

SKU-pack size numbers ending with a "3" are SmartChemicals with an RFID tag on the label for seamless data transfer to the instrument, e.g. xxxxxx1003 or xxxxxxx 4003. More information on SmartChemicals for Titration.

Analysis Note

Assay (H₂O): 9.90 - 10.10 mg/g

Legal Information

AQUASTAR is a registered trademark of Merck KGaA, Darmstadt, Germany

Pictograms

FlameExclamation mark

Signal Word

Warning

Hazard Statements

Hazard Classifications

Flam. Liq. 3 - STOT SE 3

Target Organs

Central nervous system

Storage Class Code

3 - Flammable liquids

WGK

WGK 1

Flash Point(F)

87.8 °F - Information refers to the main ingredient.

Flash Point(C)

31 °C - Information refers to the main ingredient.


Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Example:

T1503
Product Number
-
25G
Pack Size/Quantity

Additional examples:

705578-5MG-PW

PL860-CGA/SHF-1EA

MMYOMAG-74K-13

1000309185

enter as 1.000309185)

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Lot and Batch Numbers can be found on a product's label following the words 'Lot' or 'Batch'.

Aldrich Products

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Articles

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SmartChemicals enable wireless transfer of CoA data stored on an RFID tag on the consumable bottle to the titrator, reducing effort and chance for human error. Crucial data required for the application is transmitted safely, reliably and intelligently to the instrument.

Protocols

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Foodstuffs often provide a challenge for the water determination by Karl-Fischer. Instant Coffee is such a sample matrix and its water content has influence on quality and shelf life.

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

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