Z742108

Sigma-Aldrich

KitAlysis 24-well Reaction Block and Inertion Box Combination Starter Set

NACRES:
NB.51

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings

Nivel de calidad

100

Descripción general

The perfect KitAlysis Labware starter kit that combines the KitAlysis Inertion Box (Z742064) with the KitAlysis 24-Well Reaction Block and Screwdriver Set (Z742107).

Provides an inert environment to run oxygen sensitive cross-coupling reactions in a laboratory fume hood.
Designed to be used with KitAlysis High-Throughput Screening Kits.

Components:
  • Ιnertion Box
  • 24-Well Reaction Block
  • Torque Screwdriver set with bit
  • Reaction Block Replacement Screws (10ea)

Características y beneficios

Inertion Box
  • Run 24 micro-scale reactions in parallel under an inert atmosphere.
  • Provides a constant flow of inert gas over working area.
  • Easy attachment of tubing (not included) from inert gas valve on hood or stand-alone tank

24-well Reaction Block and Screwdriver Set
  • Torque Screwdriver specially designed to seal the block for minimal solvent loss while heating at elevated temperatures.
  • Torque setting prevents over-tightening and stripping of screws.
  • Includes small screwdriver to easily remove torqued screws after reaction is complete.

Información legal

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Certificado de Análisis

Certificado de origen

Artículos
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
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Multiple tools have been created to ensure your success with kit set up. Start with the more detailed guide to ensure you are comfortable with all of the steps before using the quick guides on the excel worksheet. Remember that while the technique is new, it is still organic chemistry and so the steps will seem easy once you try just one kit. It is just a new way of approaching something you are already very good at.
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The PhotoKitAlysis Reaction Kit was designed to provide the best possible chance of finding good reaction conditions for cross-coupling reactions: pre-weighed base or base solution (provided), 10–20 mmol coupling partner (user supplied), 10 mmol aryl halide substrate (user supplied), Catalysts (user supplied), 6 solvents (toluene, DMA. THJF, n-butanol, MeOH, MeCN) (provided).
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Protocolos
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
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A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.
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Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
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