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55234-U

Supel QuE QuEChERS tube

Acetate Tube, pk of 50, AOAC® 2007.01

Synonym(s):

QuEChERS

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21
Material:
polypropylene tube
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Product Name

Supel QuE, Acetate Tube, pk of 50, AOAC® 2007.01

material

polypropylene tube

Quality Level

agency

AOAC® 2007.01

product line

Supel

composition

magnesium sulfate, 6 g , sodium acetate, 1.5 g (Cat. No. 58750)

packaging

pk of 50

technique(s)

QuEChERS: suitable

centrifuge tube volume

15 mL

application(s)

food and beverages

separation technique

ion exchange

General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Application

Suitable for extracting 10-15 g food/agricultural sample. The high level of salts (e.g. magnesium sulfate) is to induce phase separation between the acetonitrile and aqueous sample layer.

Legal Information

AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC

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This Item
55295-U55294-U55173-U
material

polypropylene tube

material

polypropylene tube

material

polypropylene tube

material

-

separation technique

ion exchange

separation technique

-

separation technique

-

separation technique

-

composition

magnesium sulfate, 6 g , sodium acetate, 1.5 g (Cat. No. 58750)

composition

magnesium sulfate, 6 g , sodium chloride, 1 1/2 g

composition

magnesium sulfate, 4 g , sodium chloride, 1 g

composition

Discovery® C18, 25 mg , magnesium sulfate, 150 mg , Supelclean PSA, 25 mg

agency

AOAC® 2007.01

agency

suitable for EPA ACB B21-02, suitable for EPA ACB B23-05b

agency

-

agency

suitable for BS EN 15662:2008

packaging

pk of 50

packaging

pk of 50

packaging

pk of 50

packaging

pack of 100

Quality Level

100

Quality Level

100

Quality Level

100

Quality Level

100


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Storage Class

12 - Non Combustible Liquids

wgk

WGK 1

flash_point_f

Not applicable

flash_point_c

Not applicable



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Protocols

Analysis of banned neonicotinoid insecticides from dandelion blossoms using QuEChERS and LC-MS.

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

Related Content

Gas chromatography separates volatile compounds in the gas phase, applied in various industries for quality control.

La chromatographie en phase gazeuse sépare les composés volatils en phase gazeuse. Elle est utilisée dans diverses industries pour le contrôle qualité.

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

View All Related Content

Calogero Di Bella et al.
Frontiers in public health, 8, 273-273 (2020-08-01)
Heavy metals and PAHs were measured in animal foodstuffs from Augusta-Melilli-Priolo area in order to evaluate the potential human health risk associated to their consumption. All heavy metals were detected in seafood products while most of them were <LOD in
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)



Global Trade Item Number

SKUGTIN
55234-U04061835552436

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