KITALYSIS-SM

Sigma-Aldrich

KitAlysis 高通量Suzuki-Miyaura 交叉偶联反应筛选试剂盒 - Pack of 4

别名:
Suzuki-Miyaura 交叉偶联
NACRES:
NA.22

reaction suitability

core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings

官能团

phosphine

应用

本试剂盒用于Suzuki-Miyaura交叉偶联反应的筛选。详细的分步手册和可下载的实验用Excel模板可通过以下链接获得。
Suzuki-Miyaura交叉欧联反应筛选试剂盒详细的分步手册
可下载的实验用Excel模板

每个试剂盒包含4个可定制的筛选试剂盒,每个试剂盒包括以下试剂:
  • 6 x 4 预称重催化剂,带磁力搅拌棒顶部有盖垫的包装。
  • 1 (2 mL) ampule each of Toluene, THF, n-Butanol, DMAc, and aq. 1.5 M K3PO4.
  • 4个新的24孔反应模块替换薄膜。
  • 4个底物反应瓶,带搅拌棒。
  • 1个内参标准品。

建议与专门设计的Benchtop Inertion BoxKitAlysis 24孔反应模块(需单独订购)配合使用。

特点和优势

  • 经合成化学家严格设计和测试。
  • 轻松开展24组平行微型反应。
  • 10 μmol反应:1 μmol催化剂、3当量碱,0.1 M浓度。
  • 用于快速计算并包含电子实验记录本功能的可定制Excel模板。

法律信息

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

试剂盒组分也可单独购买

产品编号
说明
化学品安全说明书

  • 732117Pd-PEPPSI-IPent catalyst, ≥95% 5 µmol

  • 753009SPhos Pd G2 5 µmol

  • 761311cataCXium® A Pd G2 5 µmol

  • 763381XPhos Pd G3, 98% 5 µmol

  • 764175P(Cy3) Pd G3, 97% 5 µmol

  • 764183APhos Pd G3, 97% 5 µmol

  • 900522Toluene, anhydrous, ZerO2®, 99.8% 8 mL

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% 8 mL

  • 9006391-Butanol, anhydrous, ZerO2®, 99.8% 8 mL

  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% 8 mL

  • Degassed Potassium phosphate tribasic solution 8 mL

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA

  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

查看所有结果 (13)

警示用语:

Danger

hazcat

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2

靶器官

Central nervous system

补充剂危害

EUH019

storage_class_code

3 - Flammable liquids

闪点(F)

1.4 °F

闪点(C)

-17 °C

分析证书

原产地证书 (CofO)

High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in...
Karl D Collins et al.
Nature chemistry, 6(10), 859-871 (2014-09-23)
New organic reactivity has often been discovered by happenstance. Several recent research efforts have attempted to leverage this to discover new reactions. In this Review, we attempt to unify reported approaches to reaction discovery on the basis of the practical...
技术文章
All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form.
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KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
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Multiple tools have been created to ensure your success with kit set up. Start with the more detailed guide to ensure you are comfortable with all of the steps before using the quick guides on the excel worksheet. Remember that while the technique is new, it is still organic chemistry and so the steps will seem easy once you try just one kit. It is just a new way of approaching something you are already very good at.
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Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit
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实验方案
A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.
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