Merck
All Photos(1)

54341-U

Supelco

Supelclean EZ-POP NP小柱

volume 12 mL, pkg of 20

NACRES:
NB.21

物料

polypropylene tube

质量水平

产品线

Supelclean

组成

bed A, 1.25 g (Supelclean LC-Florisil®)
bed b, 1.25 g (Z-Sep/C18)

包装

pkg of 20

technique(s)

solid phase extraction (SPE): suitable

体积

12 mL

基质活性基团

C18 bonding phase
florisil bonding phase
zirconia bonding phase

application(s)

food and beverages

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52578-U

Supelclean PSA SPE 管

Supelclean™ PSA SPE Tube bed wt. 500 mg, volume 6 mL, pk of 30

Supelco

52579-U

Supelclean PSA SPE 管

material

polypropylene tube

material

PE frit (20 μm porosity), polypropylene hardware

material

PE frit (20 μm porosity), polypropylene hardware

material

PE frit (20 μm porosity), polypropylene hardware

composition

bed A, 1.25 g (Supelclean LC-Florisil®), bed b, 1.25 g (Z-Sep/C18)

composition

bed wt., 1 g

composition

bed wt., 200 mg

composition

bed wt., 500 mg

packaging

pkg of 20

packaging

pk of 30

packaging

pk of 54

packaging

pk of 30

volume

12 mL

volume

6 mL

volume

3 mL

volume

6 mL

matrix active group

C18 bonding phase, florisil bonding phase, zirconia bonding phase

matrix active group

C8 (octyl) bonding, polymerically bonded

matrix active group

ethylenediamine-N-propy bonding, polymerically bonded

matrix active group

ethylenediamine-N-propy bonding, polymerically bonded

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

一般描述

固位机制:通过正相、疏水和 Lewis 酸-Lewis 碱相互作用保留脂质基质
样品基质相容性 :油类

  • 含有 LC-Florisil ®(上层)和 Z-Sep/C18(下层)SPE 吸附剂的双层 SPE,通过 PE 熔块分离。
  • 开发用于在分析来自石油基质的非极性持久性有机污染物 (POP) 时提供优越的清理。
  • 脂肪基质优先保留在滤芯中,而非极性 POP 用乙腈清洗。

这种多床固相萃取 (SPE) 小柱设计用于从橄榄油和玉米油等食用油基质中提取非极性持久性有机污染物 (POP),特别是重和轻的多环芳烃 (PAHs)。当使用乙腈清洗多环芳烃时,脂肪基质优先保留在滤芯中。所得浸提液适用于 GC-MS 或 HPLC-FLD 分析。SPE 小柱的顶层由 Florisil ® 组成,这是一种极性吸附介质,可与极性官能团(如酸和醇)相互作用。底层由 Discovery ® DSC-18 和 Z-Sep 吸附剂组成。C18 通过疏水作用结合脂肪基质。Z-Sep 是一种氧化锆涂层二氧化硅,作为 Lewis 酸,与脂肪酸、单甘油酯和甘油二酯中的 OH 和 COOH 基团内的氧相互作用。

法律信息

Discovery is a registered trademark of Sigma-Aldrich Co. LLC
Florisil is a registered trademark of U.S. Silica Company
Supelclean is a trademark of Sigma-Aldrich Co. LLC

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(F)

Not applicable

闪点(C)

Not applicable


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