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  • [Analysis of volatile constituents in leaves of three cypress species by gas chromatography/mass spectrometry].

[Analysis of volatile constituents in leaves of three cypress species by gas chromatography/mass spectrometry].

Se pu = Chinese journal of chromatography (2006-07-13)
Dejun Hao, Yonghui Zhang, Huaguo Dai, Yan Wang
ABSTRACT

Volatile oils in leaves of three cypress species were extracted by hydrodistillation method and analyzed by gas chromatography/mass spectrometry. Sixty-four constituents were separated and identified. The majority of the components were found to be monoterpenes and sesquiterpenes. There were 33, 37, 37 compounds in the oils of leaves of Sabina chinensis (L.) Ant, Cupressus lusitanica 'zhongshan' Mill and Sabina chinensis (L.) Ant. Cv. Kaizuca, respectively. Fourteen compounds were common to them, which were thujene, alpha-pinene, camphene, sabinene, beta-myrcene, alpha-terpinene, gamma-terpinene, alpha-terpinolene, bornyl acetate, beta-elemene, alpha-amorphene, germacrene D, delta-cadinene and elemol. In addition, each species had particular compounds. The main components were found to be: sabinene (20.99%), limonene (19.78%) and bornyl acetate (11.68%) for Sabina chinensis (L.) Ant; alpha-pinene (10.39%), sabinene (11.19%) and delta-3-carene (8.88%) for Cupressus lusitanica 'zhongshan' Mill; limonene (24.56%), beta-myrcene (8.04%) for Sabina chinensis (L.) Ant. Cv. Kaizuca.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Terpinolene, ≥95%, FG
Sigma-Aldrich
3-Carene, ≥90%
Supelco
(+)-3-Carene, analytical standard
Supelco
Myrcene, analytical standard
Sigma-Aldrich
Myrcene, stabilized, FCC, FG
Sigma-Aldrich
3-Carene, 90%
Sigma-Aldrich
Myrcene, technical grade
Sigma-Aldrich
Terpinolene, technical, ≥85% (GC)
Sigma-Aldrich
(1S)-(+)-3-Carene, 99%