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Ionic Liquid GC Column Option for the Analysis of Omega 3 and Omega 6 Fatty Acids
Compared to existing ‘wax’ columns, the SLB-IL60 column offers unique selectivity, some cis/trans resolution, and faster elution for the analysis of omega 3 and omega 6 fatty acid methyl esters.
GC Analysis of a 37-Component FAME Mix on Omegawax®
This technical article will discuss GC Analysis of a 37-Component FAME Mix on Omegawax.
The Use of Derivatization Reagents for GC
The Use of Derivatization Reagents for GC
The Best Approaches to Gas Purification
The Best Approaches to Gas Purification
Resolving by Mass
Resolving by Mass
Hopane Reference Standards for use as Petrochemical Biomarkers in Oil Field Remediation and Spill Analysis
We provide high-quality, relevant hopane reference standards to be used as biomarkers for petrochemical oil field remediation and spill analysis.
New cis/trans FAME Standard for Optimising GC System Performance
AOCS and AOAC methods for determining the trans fatty acid composition of foods by gas chromatography require the use of a highly polar cyanosilicone capillary column to provide the best peak resolution attainable of the numerous geometric (cis & trans)
Resolves Difficult Sample Matrix Problems
In the flavor and fragrance industry, analytical chemists are often required to isolate key ingredients, off-flavor components, or trace organic compounds from their sample matrices without altering their structure or composition.
Analysis of Pesticides in Baby Food by Solid Phase Microextraction (SPME) Using a New Overcoated Fiber
A direct immersion SPME method using a new overcoated SPME fiber was developed for the extraction of pesticides from pureed prune baby food.
GC Injection Port Issues: Two Case Studies (Peak Tailing and Low Response)
Proper product selection and preventative maintenance for the GC inlet are vital elements that impact performance of the GC instrument.
Silylation of Non-Steroidal Anti-Inflammatory Drugs
Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs
GC Analysis of Permanent Gases and Light Hydrocarbons on Carboxen-1006 PLOT and a Packed Column (Carboxen® 1004)
Separation of Methane; Acetylene; Carbon monoxide; Water; Nitrogen; Carbon dioxide; Ethane; Ethylene
Achieve Exceptional Resolution of PAHs, Including Several Isomer Sets Using SLB®-ILPAH Capillary GC Columns
SLB®-ILPAH is a special purpose column based on an ionic liquid stationary phase providing unique selectivity and efficient column dimensions allowing exceptional resolution of PAHs
P-I-A-N-O Standards for Detailed Hydrocarbon Analyses
This is an article concerning P-I-A-N-O standards for detailed hydrocarbon analyses.
The Derivatization and Analysis of Amino Acids by GC-MS
The Derivatization and Analysis of Amino Acids by GC-MS
How to Choose a Capillary GC Column
Achieve better gas chromatography separations with an appropriate column. Review the most significant factors for gc column selection: stationary phase, internal diameter, film thickness, and column length.
Improved Recoveries and Lower Background for GC/MS/MS and LC/MS/MS Analysis of Pesticides in Green Tea
A procedure for cleanup of green tea extracts provides low background and allowed for the analysis of more pesticides at lower levels than QuEChERS. Uses less solvents and no toluene.
Comparison of QuEChERS Products for the Extraction of Planar Pesticides from Spinach
Supel™ QuE Verde combines a novel carbon with zirconia coated silica (Z-Sep+) to provide an optimum balance between planar pesticide recovery and color removal.
Method Validation for Determination of Chloramphenicol in Urine Using Molecularly Imprinted Polymer (MIP) SPE
The method for determination of low concentrations of chloramphenicol in bovine and porcine urine was developed. Sample cleanup was performed by Molecular Imprinted Polymer (MIP) columns. Confirmatory analyses were conducted using GC/MS-NCI after derivatisation (silylation). The described method was fully
Improved GC/MS Derivatization Techniques for Analysis of New Designer Drugs: Methylone, Ethylone, Butylone, Mephedrone, and Methedrone
As new “bath salt” drugs such as methylone, ethylone, mephedrone, butylone and other methcathinone analogs increase in popularity, toxicologists require native and labeled certified reference materials to accurately identify and quantify the new compounds in patient samples.
GC Analysis of Spearmint Essential Oil on SLB®-IL59
-Cymene; Linalool; Menthol; α-Terpineol; Menthyl acetate
Measuring Flows For Gas Chromatography Volumetric vs. Mass
Measuring Flows For Gas Chromatography Volumetric vs. Mass
US EPA Method 8041: GC Analysis of Phenols on Equity®-5
Separation of 2-Chlorophenol; 2,4-Dichlorophenol; 2,4,6-Tribromophenol; 2,4,6-Trichlorophenol; 2,4-Dinitrophenol; Pentafluorophenol; 2-Methylphenol, analytical standard; 2,3,4,6-Tetrachlorophenol; Pentachlorophenol; 4-Nitrophenol; 2-Bromophenol; 2,3,5,6-Tetrachlorophenol; 2,3,5-Trichlorophenol; 4-Chloro-3-methylphenol; 2,4,5-Trichlorophenol; 4-Methylphenol, analytical standard; 2,4-Dimethylphenol; 2-Nitrophenol; 3-Methylphenol, analytical standard; Phenol; 2-Methyl-4,6-dinitrophenol; 2,3,4-Trichlorophenol; 2,6-Dichlorophenol; 2,3,4,5-Tetrachlorophenol
GC Analysis of Class 3 Residual Solvents on OVI-G43
Butyl methyl ether; Acetic acid; 2-Butanone; Ethyl acetate; Tetrahydrofuran; 1-Butanol; Isopropyl acetate; Heptane; Propyl acetate; 3-Methylbutanol; 4-Methyl-2-pentanone; Isobutyl acetate; Butyl acetate; Dimethyl sulfoxide; Anisole; Cumene
GC Analysis of C2-C7 Free Fatty Acids on Nukol™
Separation of Propionic acid; Acetic acid; Heptanoic acid; Isobutyric acid; Valeric acid; Isocaproic acid; Butyric acid; Isovaleric acid
SPME Fiber Performance Tips for Volatiles & Semi-Volatiles
Enhance the extraction capability of Supelco SPME fibers for the collection of volatiles, semi-volatiles and polar compounds. spme
Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS after Cleanup with Dual-Layer SPE Cartridge
Pesticide residue testing of turmeric and other (dried) spices is challenging due to their complex compositions and high matrix. An efficient SPE clean-up can be achieved by a new Dual-layer cartridge.
GC Column Selection Guide
An optimized chromatographic separation begins with the column. Learn to select the proper capillary column based on stationary phase, column I.D., film thickness, and column length.
Solid Phase Microextraction: Frequently Asked Questions
Answers and tips relating to the application of the solid phase micro-extraction technique.
HPLC Analysis of Active Cannabinoid Compounds in Gummy Bear Candy on Ascentis® Express Biphenyl with UV Detection after Extraction
Tetrahydrocannabinolic acid A solution, 1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material.
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