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1.05721

TLC plates, Silica gel 60

pkg of 25 plates, plate L × W 20 cm × 20 cm, glass support

別名:

Silica Gel 60 TLC Plates

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この商品について

NACRES:
NB.21
UNSPSC Code:
41115711
この製品は、Merck Milliporeウェブサイトでのみ注文できます。
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Quality Level

material

glass support, silica gel 60 matrix

feature

binder Organic Polymer, fluorescent indicator: no

packaging

pkg of 25 plates

technique(s)

thin layer chromatography (TLC): suitable

layer thickness

250 μm

plate L × W

20 cm × 20 cm

particle size

10-12 μm

pore size

60 Å medium pore diameter

storage temp.

2-30°C

General description

25 Glass plates 20 x 20 cm
Our classical silica TLC plates are based on a combination of our proven silica gel 60 and the addition of a unique polymeric binder resulting in a very adherent and hard surface that will not crack or blister and even allow writing with a pensil on the surface without risk to damage the layer.

Application


  • Pressurized planar electrochromatography of DNS amino acids derivatives in silica gel and silanized silica gel systems with formic acid addition to the water mobile phase: This study explores the separation selectivity of dansyl (DNS) derivatives of amino acids using pressurized planar electrochromatography (PPEC) on Silica gel 60 TLC plates. The research demonstrates significant differences in separation selectivity between high-performance thin-layer chromatography (HPTLC) and PPEC systems, highlighting the electrophoretic effects in the PPEC system (Chomicki and Dzido, 2021).

  • Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates: This article presents investigations into the separation selectivity of DNS derivatives of amino acids on Silica gel 60 TLC plates. The study shows the impact of varying concentrations of acetonitrile in the mobile phase on the separation efficiency, providing valuable insights for optimizing analytical techniques in biochemical research (Chomicki and Dzido, 2022).

  • Determination of β-blocking receptor drugs in silica gel TLC systems with the mobile phase containing surfactant: This research examines the retention and separation of β-blocking drugs on Silica gel 60 TLC plates using mobile phases with surfactants. The study assesses the effect of surfactant concentration on zone shape properties and provides a quantitative analysis of selected solutes, emphasizing the method′s environmental friendliness due to low propanol use (Traczuk and Polak, 2022).

Analysis Note

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 9.7 - 11.7 µm
Layer thickness: 210 - 270 µm
Deviation of layer thickness per plate: ≤ 35 µm
Chromatographic testing:
colour test
hRf-values
- bleu vif organol, colour test, lipophile:
11 - 25
- Ceres Black G, colour test, lipophile: 34 - 48
- ceres Violet brn, colour test, lipophile: 52 - 67
separation number (colourtest, lipophile): ≥ 10.5
Typical value determined on a conditioned plate
Eluent: toluene (45% rel. humidity)

Other Notes

Replaces: 5721-7; 5721

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当該品目
1.056261.153261.05748
technique(s)

thin layer chromatography (TLC): suitable

technique(s)

thin layer chromatography (TLC): suitable

technique(s)

thin layer chromatography (TLC): suitable

technique(s)

thin layer chromatography (TLC): suitable

material

glass support, silica gel 60 matrix

material

glass support, silica gel 60 matrix

material

glass support, silica gel 60 matrix

material

plastic support, silica gel 60 matrix

pore size

60 Å medium pore diameter

pore size

60 Å medium pore diameter

pore size

60 Å medium pore diameter

pore size

60 Å medium pore diameter

feature

binder Organic Polymer, fluorescent indicator: no

feature

binder Organic Polymer, fluorescent indicator: no

feature

binder Organic Polymer, fluorescent indicator: no

feature

binder Organic Polymer, fluorescent indicator: no

particle size

10-12 μm

particle size

10-12 μm

particle size

10-12 μm

particle size

10-12 μm

packaging

pkg of 25 plates

packaging

pkg of 50 plates

packaging

pkg of 100 plates

packaging

pkg of 25 sheets


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資料

HPTLC plates provide superior separation, speed, and sensitivity, making them ideal for advanced qualitative and quantitative analysis.

Thin Layer Chromatography Troubleshooting: This article details TLC tips and tricks that one must consider while performing different steps of the technique.





グローバルトレードアイテム番号

カタログ番号GTIN
105721000104022536067858

質問

1–2/2 質問  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 回答
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdf

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  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 回答
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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