Merck

Reactions of organolithiums with dialkyl oxalates. A flow microreactor approach to synthesis of functionalized α-keto esters.

Chemical communications (Cambridge, England) (2013-03-15)
Aiichiro Nagaki, Daisuke Ichinari, Jun-ichi Yoshida
RESUMEN

Reactions of functionalized aryllithiums with dialkyl oxalates were achieved using a flow microreactor to obtain α-keto esters with high selectivity by virtue of fast 1 : 1 micromixing.

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Sigma-Aldrich
Bromobenzene, ReagentPlus®, 99%
Sigma-Aldrich
Bromobenzene, ≥99.5% (GC)