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28471-U

Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

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Synonym(s):
GC column, SPB-5, 5% diphenyl, mass spec
UNSPSC Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54

material

fused silica

Quality Level

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

reg. compliance

FDA LIB 4423

parameter

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Beta value

250

df

0.25 μm

technique(s)

GC/MS: suitable
gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary non-polar

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General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
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