55295-U
Supel™ QuE QuEChERS tube
Non-Buffered Tube 2, pk of 50, suitable for PFAS testing
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product name
Supel™ QuE, Non-Buffered Tube 2, pk of 50, suitable for PFAS testing
material
polypropylene tube
Quality Level
Agency
suitable for EPA ACB B21-02
suitable for EPA ACB B23-05b
reg. compliance
suitable for FDA C-010.02
product line
Supel™
composition
magnesium sulfate, 6 g
sodium chloride, 1 1/2 g
packaging
pk of 50
technique(s)
QuEChERS: suitable
centrifuge tube volume
15 mL
application(s)
food and beverages
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General description
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
Legal Information
WGK
WGK 1
Certificates of Analysis (COA)
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Articles
Discover an LC-MS/MS method for the analysis of 16 per- and polyfluoroalkyl compounds (PFAS) in milk using QuEChERS extraction technique following FDA C-010.02 guidelines.
Find more about the analysis of 16 PFAS in salmon via QuEChERS extraction and LC-MS/MS characterization following FDA Method C-010.02.
Protocols
HPLC-UV analysis of active compounds in marijuana-infused edibles for potency testing; complex matrix requires precise methods.
Rapid potency testing of marijuana-infused edibles using LC/MS on a biphenyl stationary phase detected eleven cannabinoids.
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