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Calibration, qualification, and validation
facet applications:Calibration, qualification, and validation
facet content type:Protocol
Showing 1-30 of 64 results
FAME Standard for Optimizing GC System Performance
FAME Standard for Optimizing GC System Performance
Quantitative NMR for Content Assignment of Reference Standards for Quality Control of Herbal Medicinal Products
qNMR has proven to be appropriate as a primary analytical method for the certification of natural products as reference standards for QC of herbal medicinals.
US EPA Method 8015 (modified): GC Analysis of Gasoline Range Organics (GRO) on SLB®-5ms, Direct Injection
-Xylene 1000 μg/mL; 1,2,4-Trimethylbenzene 1000 μg/mL
LC/MS (TOF) Analysis of Drugs and Their Glucuronide Metabolites in Urine on Titan™ C18 After Solid Phase Extraction (SPE) Using Supel™-Select SCX, β-Glucuronidase Enzyme Digestion
-THC solution, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material
LC/MS/MS Analysis of Aflatoxins in Cannabis on Ascentis® Express 2.7µm Phenyl-Hexyl after Cleanup Using Supel™ Tox AflaZea SPE
solution, 2 μg/mL in acetonitrile, analytical standard
Fast GC Analysis of Detailed cis/trans Fatty Acid Methyl Esters (FAMEs) on the 75 m SP™-2560 Capillary Column
Fast GC Analysis of Detailed cis/trans Fatty Acid Methyl Esters (FAMEs) on the 75 m SP™-2560 Capillary Column
GC Analysis of Bacterial Acid Methyl Esters (BAMEs) on Equity®-1
Protocol for GC Analysis of Bacterial Acid Methyl Esters (BAMEs) on Equity®-1
Fast and Reliable Environmental Analysis of Aldehyde and Ketone Air Pollutants
Aldehydes and ketones are ubiquitous air pollutants. Along with esters and ethers, they are major components of indoor air pollution and are therefore important for industrial hygiene applications.
GC Analysis of a 37-Component FAME Mix on SP™-2560
A protocol for GC Analysis of a 37-Component FAME Mix on SP™-2560.
Qualitative Thin Layer Chromatography Analysis Ginkgo
Qualitative Thin Layer Chromatography Analysis of Flavonoids and Quantification of Terpene Lactones in Ginkgo Biloba Extracts and Tablets
New GC-MS Method for Mycotoxin Analysis
An article regarding A New GC-MS Method for Mycotoxin Analysis Using 13C-marked Mycotoxin Derivatives from Sigma-Aldrich.com
EN 14105: GC Analysis of Glycerin Impurity in Biodiesel on MET-Biodiesel
EN 14105: GC Analysis of Glycerin Impurity in Biodiesel on MET-Biodiesel
MET-Biodiesel Capillary GC Column
B100 biodiesel analysis of free glycerin & total glycerin by Gas Chromatography using the Supelco MET-Biodiesel capillary gc column for ASTM D6584 & EN 14105
GC Analysis of a 37-Component FAME Mix on SP™-2560, Slower Oven Ramp
GC Analysis of a 37-Component FAME Mix on SP™-2560, Slower Oven Ramp
Accurate Biological Testing for Amphetamine and Methamphetamine Abuse Using Chiral HPLC and MS Detection
Optimized sample prep and chiral chromatography methods for the LC/MS analysis of these drug enantiomers in urine
Detection and Determination of Caffeine, Taurine and Arginine in Shampoos by HPTLC
The modern thin-layer chromatography (TLC) offers advantages also in the field of cosmetics to quickly and simultaneously analyze samples with densitometric detection.
Analytical Standards of Boswellic Acids and Their Separation
We offer six boswellic acids as analytical standards and two neat standards of α+β mixtures for use in research and quality control.
Analysis of Active Cannabis Compounds (Cannabinoids) in Edible Food Products: Gummy Bears and Brownies
Rapid potency testing of marijuana-infused edibles using LC/MS on a biphenyl stationary phase detected eleven cannabinoids.
Rapid, Sensitive, and Quantitative LC/MS/MS Determination of Digitoxin and Digoxin in Plasma
Immunoassay-based methods for digitoxin or digoxin exist, but are time consuming, labor intensive, and not selective due to similarities in their chemical structures.
LC/MS/MS Analysis of Steroid Hormones in Plasma
The conversion of clinical methods to LC/MS/MS offers advantages; however, is accompanied by a few limitations, notably interference effects from the endogenous sample matrix.
Chiral and Achiral LC-MS Analysis of Warfarin™ in Plasma Samples
This study demonstrates the analysis of Warfarin in plasma samples utilizing chiral and achiral (reversed-phase) LC-MS and effective sample prep to remove endogenous phospholipids
Analysis of Fipronil and Fipronil Sulfone in Eggs, Chicken Meat and Mayonnaise
A short abstract on a method using QuEChERS and GC/MS/MS for determination of fipronil & fipronil sulfone.
Analysis of Residual Solvents in Hemp Extracts
SPME enables rapid, sensitive GC/MS analysis of residual solvents in hemp extract, ensuring accuracy and efficiency.
Hydrocarbon Oil Index in Samples
Special mineral oil standard mixtures are gravimetrically produced for calibration.
Analysis of Active Cannabis Compounds
HPLC-UV analysis of active compounds in marijuana-infused edibles for potency testing; complex matrix requires precise methods.
UHPLC/MS for Drug Detection in Urine
Optimize β-glucuronidase hydrolysis for glucuronide metabolite analysis considering factors like time, temperature, pH, and enzyme concentration.
Complete Workflow for Comprehensive Cannabis Terpenes Analysis
Complete workflow for the comprehensive analysis of terpenes in cannabis
Fast GC for Trans FAME Analysis
Fast GC analysis utilizes short capillary columns, H2 carrier gas, and rapid temperature programming rates.
Determination of Caffeine in Coffee Using High Performance Thin Layer Chromatography
HPTLC was used to analyze caffeine in coffee. Filtration of coffee through a PTFE syringe filter was the only sample preparation. Quantitation was conducted with a TLC scanner.
Determination of Quinine in Tonic Water and Caffeine in Coffee and Cola Drinks Using TLC-MS
HPTLC–MS analysis of quinine in tonic water and caffeine in coffee and cola drinks.
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