Merck
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69479

Supelco

N-Methyl-N-(trimethylsilyl)trifluoroacetamide

for GC derivatization, LiChropur, ≥98.5%

Synonym(s):
N-Trimethylsilyl-N-methyl trifluoroacetamide, MSTFA
Linear Formula:
CF3CON(CH3)Si(CH3)3
CAS Number:
Molecular Weight:
199.25
Beilstein:
1941550
Numer EC:
Numer MDL:
Identyfikator substancji w PubChem:
NACRES:
NA.22

klasa czystości

for GC derivatization

Poziom jakości

100

gęstość pary

>1 (vs air)

ciśnienie pary

8.8 mmHg ( 27 °C)

próba

≥98.5% (GC)
≥98.5%

forma

liquid

jakość

LiChropur

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

technique(s)

gas chromatography (GC): suitable

współczynnik refrakcji

n20/D 1.38 (lit.)
n20/D 1.380

tw

130-132 °C (lit.)

gęstość

1.075 g/mL at 25 °C (lit.)

temp. przechowywania

2-8°C

SMILES string

CN(C(=O)C(F)(F)F)[Si](C)(C)C

InChI

1S/C6H12F3NOSi/c1-10(12(2,3)4)5(11)6(7,8)9/h1-4H3

InChI key

MSPCIZMDDUQPGJ-UHFFFAOYSA-N

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Opis ogólny

N-Methyl-N-(trimethylsilyl)trifluoroacetamide (MSTFA) is a silylating reagent.[1]

Zastosowanie

Learn more in the Product Information
MSTFA may be used in silylation procedure to detemine steroid hormones 17α-ethinylestradiol (EE2) and estrone using GC-MS. MSTFA along with Trimethylsilyl chloride (TMCS) in eithyl acetate, acetonitrile and dichloromethane solvents leads to formation of trimethylsilyl (TMS) and tert-butyldimethylsilyl (TBS) derivatives.[1]
Suitable for the derivatization of amines, amino acids, carboxyl, hydroxyamines, indolalkylamine, n-nitrosoamino acids, nucleosides, phenolalkylamines, serotonin and tryptamine.

Inne uwagi

Powerful silylating agent[2][3][4][5]
Reagent for N-acetyl-N, trifluoroacetyl, trimethylsilyl, N-trimethylsilyl-N-trifluoroacetyl, and O-trimethylsilyl (TMS)

Informacje prawne

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

piktogramy

FlameExclamation mark

Hasło ostrzegawcze

Warning

Zwroty wskazujące rodzaj zagrożenia

Klasyfikacja zagrożeń

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3

Organy docelowe

Respiratory system

Kod klasy składowania

3 - Flammable liquids

WGK

WGK 3

Temperatura zapłonu °F

77.0 °F - closed cup

Temperatura zapłonu °C

25 °C - closed cup

Środki ochrony indywidualnej

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

Certificate of Analysis

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Certificate of Origin

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