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Z742680

Sigma-Aldrich

SynLED Parallel Photoreactor

AC/DC input

, universal plug set (included)
100 - 240 V AC, 50/60 Hz

feature

capacity 16  vial(s)

reaction suitability

reagent type: catalyst
reaction type: Photocatalysis

parameter

465-470 nm spectral range

General description

This newly designed photoreactor enables simple small-scale photocatalysis reaction screening ensuring high levels of consistency across reactions and between runs.

Features and Benefits

  • Bottom-lit LEDs (465-470 nm) across a 4x4 reaction block array provides consistent light intensity (130-140 lm) and angle (45°)
  • Built-in cooling fan provides consistent temperature to each parallel reaction
  • Uses 1-2 dram scintillation vials or microwave vials (O.D. of 1.7 cm or less)
  • Power supply is wall plug power supply 700mA 12 W
  • Compatible with IKA magnetic stirrer with round plate (Z645052)
  • Compatible with liquid scintillation vials (8 mL Wheaton, Z188719)

Certificate of Analysis

Certificate of Origin

Articles
Csp2- and Csp-hybridized coupling reactions are established catalytic approaches. However, multi-step Csp3- and Csp2-coupling reactions of boronic acids and related derivatives are still limited by ineffective two-electron transmetalation reactions.
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The application of radical chemistry towards organic synthesis is well-developed and wide-reaching, though often hampered by a dependence on toxic radical initiators.
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While Markovnikov alkene reactivity is very well developed and utilized commonly in the synthesis of commodity and research chemicals, catalytic access to the anti-Markovnikov-selective adducts is a much less-developed endeavor.
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Photoredox catalysis is a powerful synthetic methodology to form challenging covalent bonds using light irradiation. It is effective for light-driven polymer and small molecule synthesis.
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