06300

Supelco

Aluminum oxide

activated, neutral, Brockmann Activity I

Synonym(s):
Alumina
Linear Formula:
Al2O3
CAS Number:
Molecular Weight:
101.96
EC Number:
MDL number:
eCl@ss:
38120402
PubChem Substance ID:
NACRES:
SB.52

grade

standard

form

powder

quality

activated, neutral

application(s)

LPLC: suitable

matrix

Aluminum oxide

matrix active group

aluminum oxide

particle size

0.05-0.15 mm

pore size

60 Å mean pore size

surface area

155 m2/g

pH

7.0±0.5

mp

2040 °C (lit.)

separation technique

hydrophilic interaction (HILIC)

SMILES string

O=[Al]O[Al]=O

InChI

1S/2Al.3O

InChI key

TWNQGVIAIRXVLR-UHFFFAOYSA-N

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General description

Brockmann aluminum oxides are suitable for column chromatography and adsorptive filtration.
Aluminum oxides are generally used as solid support phases in solid phase extraction (SPE)-based clean-up procedures employed in chromatographic methods.

Application

Aluminum oxide has been used as a chromatographic column support for the purification of sn-2 monopalmitin prior to its determination by high performance liquid chromatography-evaporative light scattering detection (HPLC-ELSD).
It may be used for purification of fish tissue extract followed by liquid−liquid extraction into dichloromethane prior to the analysis for triarylmethane and phenothiazine dyes by liquid chromatography-tandem mass spectrometry (LC−MS/MS). It may also be used as a solid support phase for SPE-based analysis of pyrethroid insecticide residues in vegetable oils by gas chromatography-tandem mass spectrometry (GC-MS/MS).

storage_class_code

11 - Combustible Solids

WGK Germany

nwg

Flash Point F

Not applicable

Flash Point C

Not applicable

Personal Protective Equipment

dust mask type N95 (US),Eyeshields,Gloves

Certificate of Analysis

Certificate of Origin

Multiresidue determination of triarylmethane and phenothiazine dyes in fish tissues by LC-MS/MS.
Tarbin JA, et al.
Analytica Chimica Acta, 625(2), 188-194 (2008)
Determination of pyrethroid insecticide residues in vegetable oils by using combined solid-phases extraction and tandem mass spectrometry detection.
Esteve-Turrillas FA, et al.
Analytica Chimica Acta, 553(1-2), 50-57 (2005)
A López-López et al.
Journal of chromatography. B, Biomedical sciences and applications, 760(1), 97-105 (2001-08-28)
An alternative method to determine the sn-2 monopalmitin in infant formulas was developed and validated. This method offers many advantages over the traditional methods. It follows the official method in the first steps, purification of the fat or oil through...
Chien-Chih Lin et al.
Nanoscale, 5(17), 8090-8097 (2013-07-25)
We demonstrated a promising route for enhancing temperature sensitivity, improving saturation voltage, and reducing power consumption of the MOS(p) tunneling temperature sensors by introducing ultrathin Al2O3 into the dielectric stacks. Detailed illustrations of the working mechanism and device concept are...
Yi Tian et al.
Journal of the American Chemical Society, 136(36), 12784-12793 (2014-08-19)
Organic neutral radicals have long fascinated chemists with a fundamental understanding of structure-reactivity relationships in organic reactions and with applications as new functional materials. However, the elusive nature of these radicals makes the synthesis, isolation, and characterization very challenging. In...

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