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Solid phase microextraction
facet applications:Solid phase microextraction
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Rapid Determination of Protein Binding Affinity Using Solid Phase Microextraction
Accurate protein binding affinities were measured using bioSPME more rapidly than membrane dialysis (RED) techniques. Binding affinities correlated to the reference values.
Resolves Difficult Sample Matrix Problems
In the flavor and fragrance industry, analytical chemists are often required to isolate key ingredients, off-flavor components, or trace organic compounds from their sample matrices without altering their structure or composition.
Bioanalysis with SPME
Biocompatible SPME devices employ C18 bonded porous silica sorbent particles, in a binder which resists fouling by biological matrix components
SPME Fiber Performance Tips for Volatiles & Semi-Volatiles
Enhance the extraction capability of Supelco SPME fibers for the collection of volatiles, semi-volatiles and polar compounds. spme
Determination of 2-Chloroethanol as Marker for Fumigant Ethylene Oxide in Sesame Seeds by HS-SPME-GC-MS
The work describes the development of an HS-SPME-GC-MS method to determine 2-chloroethanol as a marker of fumigant ethylene oxide in different kinds of sesame seed samples.
Optimizing Serum Sample Preparation for Free Testosterone Determination: A Comparative Analysis Using BioSPME
Optimize serum samples for LC-MS/MS-based free testosterone determination using Supel™ BioSPME 96-pin device and validated equilibrium dialysis methods.
Analysis of Pesticides in Baby Food by Solid Phase Microextraction (SPME) Using a New Overcoated Fiber
A direct immersion SPME method using a new overcoated SPME fiber was developed for the extraction of pesticides from pureed prune baby food.
BioSPME for Plasma Protein Binding Assay: Details of Method Development and Optimization
Determination of plasma protein binding using a SupelTM C18 pin device based BioSPME method for efficient sample preparation, along with a comparison to the equilibrium dialysis method.
Speed, Simplicity and Accuracy of Protein Binding Determination using BioSPME
Learn about Supel™ BioSPME C18 high-throughput devices to determine plasma protein binding and decrease the sample preparation time to less than an hour.
SPME Adsorbent Fibers on Nitinol Core for Improved Fiber Reproducibility
A comparison between Carboxen®/PDMS coated nitinol core and fused silica core adsorbent SPME fibers for factors, such as coating process, testing process, inertness, raw materials, and durability.
SPME in the Analysis of Illicit Drugs
SPME is used in the analysis of amphetamine compounds by doing pre-extraction derivatization, and is also used in general determinations of other drugs of abuse.
GC/MS/MS Analysis of BPA in Energy Drink
Study demonstrates SPME of BPA from an energy drink using an overcoated PDMS/DVB fiber, followed by GC/MS/MS analysis.
Analysis of Tetrahydrocannabinol (THC) and Carboxytetrahydrocannabinol (THCCOOH) in Surface Waters by SPME and GC/MS
Analysis of Tetrahydrocannabinol (THC) and Carboxytetrahydrocannabinol (THCCOOH) in Surface Waters by SPME and GC/MS
Selecting the Appropriate SPME Fiber Coating –Effect of Analyte Molecular Weight and Polarity
Selecting the Appropriate SPME Fiber Coating –Effect of Analyte Molecular Weight and Polarity
Automated Solid Phase Microextraction (SPME) Sampling
Use the full range of Supelco® SPME fibers with your PAL autosampler system so you can sample smarter
Solid Phase Microextraction: Frequently Asked Questions
Answers and tips relating to the application of the solid phase micro-extraction technique.
Validation of a Simple Method for the Alcohol Content in Kombucha Tea by Headspace SPME and GC-MS
Development and validation of a headspace SPME and GC-MS method to determine alcohol content in twenty different Kombucha tea samples.
Biodiesel
Learn more about Biodiesel as a renewable, alternative diesel fuel produced from vegetable oils, animal fats, or recycled restaurant grease.
Headspace-SPME as a Versatile Monitoring Method for Early Detection of Insect Infestation in Rice
Discover a high-throughput HS-SPME-GC-MS method for detecting early insect biomarkers in rice. Utilizing a Carboxen®-PDMS phase on a nitinol fiber core ensures robustness and reproducibility in extraction and desorption processes.
Protein Binding Determination - Comparison Study of Techniques & Devices
Comparative analysis of Supel™ BioSPME 96-Pin device with a rapid equilibrium dialysis technique for accuracy of measured values, sample cleanliness, and workflow time in drug protein binding.
Multiclass Pesticide Analysis of Soy Milk Using a Matrix-Compatible SPME Fiber
Pesticide analysis, SPME Fiber, supelco spme fiber, direct immersion spme, pesticide analysis methods, pesticide analysis by gc-ms, DI-SPME, overcoated SPME, overcoated fibers, soy milk analysis
Rugged SPME Sampling
SPME fibers with CAR/PDMS and PDMS/DVB coatings on nitinol core assembly enhance fiber performance for solid phase microextraction.