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Merck

8.55003

Sigma-Aldrich

Rink Amide MBHA树脂(100-200目)

Novabiochem®

别名:

Rink Amide MBHA树脂(100-200目)

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About This Item

CAS Number:
MDL號碼:
分類程式碼代碼:
12352111
NACRES:
NA.22

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品質等級

產品線

Novabiochem®

形狀

beads

反應適用性

reaction type: Fmoc solid-phase peptide synthesis

製造商/商標名

Novabiochem®

應用

peptide synthesis

官能基

amine

儲存溫度

2-30°C

SMILES 字串

N(C(c7c(cc(cc7)OC)OC)c4ccc(cc4)OCC(=O)NC(c6ccc(cc6)C)c5ccc(cc5)C)C(=O)OCC1c2c(cccc2)c3c1cccc3

InChI

1S/C47H44N2O6/c1-30-13-17-32(18-14-30)45(33-19-15-31(2)16-20-33)48-44(50)29-54-35-23-21-34(22-24-35)46(41-26-25-36(52-3)27-43(41)53-4)49-47(51)55-28-42-39-11-7-5-9-37(39)38-10-6-8-12-40(38)42/h5-27,42,45-46H,28-29H2,1-4H3,(H,48,50)(H,49,51)

InChI 密鑰

JDDWRLPTKIOUOF-UHFFFAOYSA-N

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8.550048.551308.55001
reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

product line

Novabiochem®

product line

Novabiochem®

product line

Novabiochem®

product line

Novabiochem®

functional group

amine

functional group

amine

functional group

amine

functional group

amine

Quality Level

400

Quality Level

400

Quality Level

400

Quality Level

400

application(s)

peptide synthesis

application(s)

peptide synthesis

application(s)

peptide synthesis

application(s)

peptide synthesis

storage temp.

2-30°C

storage temp.

2-30°C

storage temp.

2-30°C

storage temp.

2-30°C

一般說明

该支持物包括通过正亮氨酸连接至MBHA树脂的修饰的Rink酰胺接头,并且是肽酰胺Fmoc SPP的理想工具。可以通过用95% TFA进行单步处理来实现从该树脂的裂解,从而以高收率和纯度提供肽酰胺。

相关方案和技术文章
肽合成用树脂的上样方案

應用


  • 用于法医学分析的液相色谱-串联质谱法:LSD-D₃可用作液相色谱-串联质谱法测定法中的内标物,用于测定法医学样品中的LSD及其代谢物,该方法提高了分析结果的准确性和精密度(Johansen and Jensen, 2005)。

  • 尿液检测中的同位素稀释质谱法:在高效液相色谱-同位素稀释质谱(IDMS)法中,研究人员以LSD-D 3为关键内标物,来定量测定尿液中的麦角酸酰二乙胺(LSD),该方法有助于我们进行精准的药物检测(White et al., 1999)。

  • 自动提取和LC/MS/MS验证:研究人员可以用LSD-D₃进行各种生物基质中麦角酸酰二乙胺的自动提取,然后使用LC/MS/MS进行验证。该应用突显了LSD-D₃提高毒理学分析效率和可靠性的作用(de Kanel et al., 1998)。

聯結

替代品:01-64-0037

分析報告

颜色(目测):白色至浅黄色至米黄色
物质外观(目测):微珠
负载量(光度法测定DBU/DMF处理后释放的Fmoc生色团):0.40 - 0.90 mmol/g
TNBS检验:符合检验
溶胀体积(DMF):结果因批次而异
溶胀体积(CH₂Cl₂):结果因批次而异
根据Houben Weyl得到的总溶胀体积(CH2Cl2): ≥ 5.2 ml/g
根据Houben Weyl得到的总溶胀体积(DMF): ≥ 5.2 ml/g
聚合物基质为共聚物(苯乙烯-1% DVB),100 - 200目。

法律資訊

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

儲存類別代碼

11 - Combustible Solids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable


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Questions

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  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Helpful?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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