If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf
8.55003
Rink Amide MBHA树脂（100-200目）
Novabiochem®
别名:
Rink Amide MBHA树脂（100-200目）
品質等級
產品線
Novabiochem®
形狀
beads
反應適用性
reaction type: Fmoc solid-phase peptide synthesis
製造商／商標名
Novabiochem®
應用
peptide synthesis
官能基
amine
儲存溫度
2-30°C
SMILES 字串
N(C(c7c(cc(cc7)OC)OC)c4ccc(cc4)OCC(=O)NC(c6ccc(cc6)C)c5ccc(cc5)C)C(=O)OCC1c2c(cccc2)c3c1cccc3
InChI
1S/C47H44N2O6/c1-30-13-17-32(18-14-30)45(33-19-15-31(2)16-20-33)48-44(50)29-54-35-23-21-34(22-24-35)46(41-26-25-36(52-3)27-43(41)53-4)49-47(51)55-28-42-39-11-7-5-9-37(39)38-10-6-8-12-40(38)42/h5-27,42,45-46H,28-29H2,1-4H3,(H,48,50)(H,49,51)
InChI 密鑰
JDDWRLPTKIOUOF-UHFFFAOYSA-N
1 of 4
此商品 | 8.55004 | 8.55130 | 8.55001 |
|---|---|---|---|
| reaction suitability reaction type: Fmoc solid-phase peptide synthesis | reaction suitability reaction type: Fmoc solid-phase peptide synthesis | reaction suitability reaction type: Fmoc solid-phase peptide synthesis | reaction suitability reaction type: Fmoc solid-phase peptide synthesis |
| product line Novabiochem® | product line Novabiochem® | product line Novabiochem® | product line Novabiochem® |
| functional group amine | functional group amine | functional group amine | functional group amine |
| Quality Level 400 | Quality Level 400 | Quality Level 400 | Quality Level 400 |
| application(s) peptide synthesis | application(s) peptide synthesis | application(s) peptide synthesis | application(s) peptide synthesis |
| storage temp. 2-30°C | storage temp. 2-30°C | storage temp. 2-30°C | storage temp. 2-30°C |
一般說明
相关方案和技术文章
肽合成用树脂的上样方案
應用
- 用于法医学分析的液相色谱-串联质谱法：LSD-D₃可用作液相色谱-串联质谱法测定法中的内标物，用于测定法医学样品中的LSD及其代谢物，该方法提高了分析结果的准确性和精密度（Johansen and Jensen, 2005）。
- 尿液检测中的同位素稀释质谱法：在高效液相色谱-同位素稀释质谱（IDMS）法中，研究人员以LSD-D 3为关键内标物，来定量测定尿液中的麦角酸酰二乙胺（LSD），该方法有助于我们进行精准的药物检测（White et al., 1999）。
- 自动提取和LC/MS/MS验证：研究人员可以用LSD-D₃进行各种生物基质中麦角酸酰二乙胺的自动提取，然后使用LC/MS/MS进行验证。该应用突显了LSD-D₃提高毒理学分析效率和可靠性的作用(de Kanel et al., 1998)。
聯結
分析報告
物质外观（目测）：微珠
负载量（光度法测定DBU/DMF处理后释放的Fmoc生色团）：0.40 - 0.90 mmol/g
TNBS检验：符合检验
溶胀体积（DMF）：结果因批次而异
溶胀体积（CH₂Cl₂）：结果因批次而异
根据Houben Weyl得到的总溶胀体积（CH2Cl2）： ≥ 5.2 ml/g
根据Houben Weyl得到的总溶胀体积（DMF）： ≥ 5.2 ml/g
聚合物基质为共聚物（苯乙烯-1% DVB），100 - 200目。
法律資訊
儲存類別代碼
11 - Combustible Solids
水污染物質分類（WGK）
WGK 3
閃點（°F）
Not applicable
閃點（°C）
Not applicable
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How is shipping temperature determined? And how is it related to the product storage temperature?
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Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf
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