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  • Versatile system for the temperature-controlled preparation of oxide crystal surfaces.

Versatile system for the temperature-controlled preparation of oxide crystal surfaces.

The Review of scientific instruments (2012-06-07)
H H Pieper, C Lammers, L Tröger, S Bahr, M Reichling
摘要

We present a versatile system for the preparation of oxide crystal surfaces in the ultra-high vacuum (UHV) at temperatures up to 1300 K. Thermal treatment is accomplished by direct current heating of a tantalum foil in contact with the oxide sample. The sample temperature is measured by a thermocouple at a position close to the crystal and its reading is calibrated against the surface temperature determined by a second thermocouple temporarily attached to the surface. The design of the sample holder is based on a transferable plate originally developed for a commercial UHV scanning probe microscope. The system is, however, also suitable for the use with electron spectroscopy or electron diffraction based surface analytical techniques. We present results for the high-temperature preparation of CeO(2)(111) surfaces with atomically flat terraces exhibiting perfect atomic order and cleanliness as revealed by non-contact atomic force microscopy (NC-AFM) imaging. NC-AFM imaging is, furthermore, used to demonstrate the temperature-controlled aggregation of gold atoms on the CeO(2)(111) surface and their evaporation at high temperatures.

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钽, foil, 100x100mm, thickness 0.100mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.0125mm, 99.9%
钽, foil, 100x100mm, thickness 0.125mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.05mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.075mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.100mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.125mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.15mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.20mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.25mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.25mm, annealed, 99.99%
钽, foil, 10mm disks, thickness 0.5mm, annealed, 99.9%
钽, foil, 10mm disks, thickness 0.75mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.006mm, 99.9%
钽, foil, 15mm disks, thickness 0.0075mm, 99.9%
钽, foil, 15mm disks, thickness 0.009mm, 99.9%
钽, foil, 15mm disks, thickness 0.0125mm, 99.9%
钽, foil, 15mm disks, thickness 0.015mm, 99.9%
钽, foil, 15mm disks, thickness 0.01mm, 99.9%
钽, foil, 15mm disks, thickness 0.025mm, as rolled, 99.9%
钽, foil, 15mm disks, thickness 0.02mm, 99.9%
钽, foil, 15mm disks, thickness 0.034mm, as rolled, 99.9%
钽, foil, 15mm disks, thickness 0.03mm, as rolled, 99.9%
钽, foil, 15mm disks, thickness 0.05mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.075mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.100mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.125mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.15mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.20mm, annealed, 99.9%
钽, foil, 15mm disks, thickness 0.25mm, annealed, 99.9%