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MilliporeSigma

250996

2-Chloro-N,N-diethylacetamide

97%

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About This Item

Linear Formula:
ClCH2CON(C2H5)2
CAS Number:
2315-36-8
Molecular Weight:
149.62
NACRES:
NA.22
PubChem Substance ID:
24855091
UNSPSC Code:
12352100
EC Number:
219-019-2
MDL number:
MFCD00000928
Assay:
97%
Form:
liquid

Key Documents

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Product Name

2-Chloro-N,N-diethylacetamide, 97%

InChI key

CQQUWTMMFMJEFE-UHFFFAOYSA-N

InChI

1S/C6H12ClNO/c1-3-8(4-2)6(9)5-7/h3-5H2,1-2H3

SMILES string

CCN(CC)C(=O)CCl

assay

97%

form

liquid

refractive index

n20/D 1.47 (lit.)

bp

148-150 °C/55 mmHg (lit.)

density

1.089 g/mL at 25 °C (lit.)

application(s)

agriculture
environmental

Quality Level

100

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This Item
24350362425137529
2-Chloro-N,N-diethylacetamide 97%

Sigma-Aldrich

250996

2-Chloro-N,N-diethylacetamide

2-Chloro-N,N-dimethylacetamide ≥97.0% (GC)

Sigma-Aldrich

24350

2-Chloro-N,N-dimethylacetamide

2-Chloro-N-methoxy-N-methylacetamide 98%

Sigma-Aldrich

362425

2-Chloro-N-methoxy-N-methylacetamide

N,N-Diethylacetamide 97%

Sigma-Aldrich

137529

N,N-Diethylacetamide

assay

97%

assay

≥97.0% (GC)

assay

98%

assay

97%

Quality Level

100

Quality Level

100

Quality Level

100

Quality Level

100

refractive index

n20/D 1.47 (lit.)

refractive index

n20/D 1.479

refractive index

-

refractive index

n20/D 1.440 (lit.)

form

liquid

form

liquid

form

solid

form

liquid

bp

148-150 °C/55 mmHg (lit.)

bp

-

bp

-

bp

182-186 °C (lit.)

density

1.089 g/mL at 25 °C (lit.)

density

1.182 g/mL at 20 °C (lit.)

density

-

density

0.925 g/mL at 25 °C (lit.)

Application

2-Chloro-N,N-diethylacetamide has been used in:
  • preparation of calixarene amides[1]
  • synthesis of 5-bromo-25,26,27,28-tetrakis[(N,N-diethylaminocarbonyl)-methoxy]calix[4]arene[2]
  • synthesis of amide calix[4]pyrrole macrocycles with super-extended cavities[3]
  • microwave-assisted organic synthesis of 3-cyano-N,N-diethyl-4-(4-methoxyphenoyl)-4-oxobutanamide[4]

pictograms

Skull and crossbones
GHS06

signalword

Danger

Hazard Classifications

Acute Tox. 1 Inhalation - Acute Tox. 3 Dermal - Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

target_organs

Respiratory system

Storage Class

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

wgk

WGK 3

flash_point_f

235.4 °F - closed cup

flash_point_c

113 °C - closed cup

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

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Certificates of Analysis (COA)

Lot/Batch Number
STBJ7566
STBF6293V
STBB6920
S42809
S36786

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[Data on hygienic standardization of N,N-diethyl-2-chloroacetamide in the air of the work area].
V A Shugaev et al.
Gigiena truda i professional'nye zabolevaniia, (6)(6), 36-37 (1991-01-01)
Dewei Tang et al.
Tetrahedron letters, 51(35), 4595-4598 (2010-08-07)
We herein report a dramatically improved total synthesis of the high-affinity translocator protein (TSPO) ligand DPA-714, featuring microwave-assisted organic synthesis (MAOS). Compared with previously described approaches, our novel MAOS method dramatically reduces overall reaction time without adversely effecting reaction yields.
Synthesis and properties of new calixarene-based ditopic receptors for the simultaneous complexation of cations and carboxylate anions.
Pelizzi N, et al.
J. Chem. Soc. Perkin Trans. II, 6, 1307-1312 (1998)
[Local and skin resorptive action of N,N-diethylchloracetamide].
V A Shugaev et al.
Gigiena truda i professional'nye zabolevaniia, (2)(2), 51-52 (1989-01-01)
Christopher J Woods et al.
Journal of the American Chemical Society, 124(29), 8644-8652 (2002-07-18)
A new "super-extended cavity" tetraacetylcalix[4]pyrrole derivative was synthesized and characterized, and X-ray crystal structures of complexes bound to fluoride and acetonitrile were obtained. The binding behavior of this receptor was investigated by NMR titration, and the complex was found to
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