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250996

Sigma-Aldrich

2-Chloro-N,N-diethylacetamide

97%

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Linear Formula:
ClCH2CON(C2H5)2
CAS Number:
2315-36-8
Molecular Weight:
149.62
EC Number:
219-019-2
MDL number:
MFCD00000928
PubChem Substance ID:
24855091
NACRES:
NA.22

Quality Level

100

Assay

97%

form

liquid

refractive index

n20/D 1.47 (lit.)

bp

148-150 °C/55 mmHg (lit.)

density

1.089 g/mL at 25 °C (lit.)

application(s)

agriculture
environmental

SMILES string

CCN(CC)C(=O)CCl

InChI

1S/C6H12ClNO/c1-3-8(4-2)6(9)5-7/h3-5H2,1-2H3

InChI key

CQQUWTMMFMJEFE-UHFFFAOYSA-N

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1 of 4

This Item
8.2039924350362425
2-Chloro-N,N-diethylacetamide 97%

Sigma-Aldrich

250996

2-Chloro-N,N-diethylacetamide

2-Chloro-N,N-diethylacetamide for synthesis

Sigma-Aldrich

8.20399

2-Chloro-N,N-diethylacetamide

2-Chloro-N,N-dimethylacetamide ≥97.0% (GC)

Sigma-Aldrich

24350

2-Chloro-N,N-dimethylacetamide

2-Chloro-N-methoxy-N-methylacetamide 98%

Sigma-Aldrich

362425

2-Chloro-N-methoxy-N-methylacetamide

form

liquid

form

liquid

form

liquid

form

solid

refractive index

n20/D 1.47 (lit.)

refractive index

-

refractive index

n20/D 1.479

refractive index

-

bp

148-150 °C/55 mmHg (lit.)

bp

114-116 °C/23 hPa

bp

-

bp

-

density

1.089 g/mL at 25 °C (lit.)

density

1.09 g/cm3 at 20 °C

density

1.182 g/mL at 20 °C (lit.)

density

-

application(s)

agriculture
environmental

application(s)

-

application(s)

-

application(s)

-

Application

2-Chloro-N,N-diethylacetamide has been used in:
  • preparation of calixarene amides
  • synthesis of 5-bromo-25,26,27,28-tetrakis[(N,N-diethylaminocarbonyl)-methoxy]calix[4]arene
  • synthesis of amide calix[4]pyrrole macrocycles with super-extended cavities
  • microwave-assisted organic synthesis of 3-cyano-N,N-diethyl-4-(4-methoxyphenoyl)-4-oxobutanamide

Pictograms

Skull and crossbones
GHS06

Signal Word

Danger

Hazard Classifications

Acute Tox. 1 Inhalation - Acute Tox. 3 Dermal - Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

Target Organs

Respiratory system

Storage Class Code

6.1A - Combustible, acute toxic Cat. 1 and 2 / very toxic hazardous materials

WGK

WGK 3

Flash Point(F)

235.4 °F - closed cup

Flash Point(C)

113 °C - closed cup

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Certificates of Analysis (COA)

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Dewei Tang et al.
Tetrahedron letters, 51(35), 4595-4598 (2010-08-07)
We herein report a dramatically improved total synthesis of the high-affinity translocator protein (TSPO) ligand DPA-714, featuring microwave-assisted organic synthesis (MAOS). Compared with previously described approaches, our novel MAOS method dramatically reduces overall reaction time without adversely effecting reaction yields.
[Data on hygienic standardization of N,N-diethyl-2-chloroacetamide in the air of the work area].
V A Shugaev et al.
Gigiena truda i professional'nye zabolevaniia, (6)(6), 36-37 (1991-01-01)
[Local and skin resorptive action of N,N-diethylchloracetamide].
V A Shugaev et al.
Gigiena truda i professional'nye zabolevaniia, (2)(2), 51-52 (1989-01-01)
Synthesis and properties of new calixarene-based ditopic receptors for the simultaneous complexation of cations and carboxylate anions.
Pelizzi N, et al.
J. Chem. Soc. Perkin Trans. II, 6, 1307-1312 (1998)
[Gas-chromatographic analysis of N,N-diethylchloracetamide in the air].
L P Shcherbakov et al.
Gigiena i sanitariia, (5)(5), 57-59 (1989-05-01)
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