MilliporeSigma
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1.05735

Supelco

TLC Silica gel 60 F₂₅₄

pkg of 25 sheets, sheet L × W 20 cm × 20 cm, plastic support

material

plastic support
silica gel 60 matrix

Quality Level

feature

binder Organic Polymer
fluorescent indicator

packaging

pkg of 25 sheets

technique(s)

thin layer chromatography (TLC): suitable

layer thickness

200 μm

sheet L × W

20 cm × 20 cm

particle size

10-12 μm

pore size

60 Å medium pore diameter

storage temp.

2-30°C

General description

25 Plastic sheets 20 x 20 cm
Our classical silica TLC plates are based on a combination of our proven silica gel 60 and the addition of a unique polymeric binder resulting in a very adherent and hard surface that will not crack or blister and even allow writing with a pencil on the surface without risk to damage the layer.

Linkage

Replaces: 5735-7; 5735

Analysis Note

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 9.5 - 11.5 µm
Layer thickness: 175 - 225 µm
Deviation of layer thickness per plate: ≤ 40 µm
Chromatographic testings:
A) Colour test
hRf-values
- bleu vif organol, colour test, lipophile:
11 - 25
- Ceres Black G, colour test, lipophile: 34 - 48
- ceres Violet brn, colour test, lipophile: 52 - 67
separation number (colourtest, lipophile): ≥ 10.5
B) Steriod test
hRf-values
- hydrocortisone, steroid test:
25 - 37
- Reichstein S, steroid test: 37 - 49
- methyltestosterone, steroid test: 42 - 54
Typical value determined on a conditioned sheet
Eluent A) Toluene (45% rel.humidity)
Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel.humidity)

Certificate of Analysis

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Certificate of Quality

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