For information on the use of phenacyl bromide to derivatize carboxylic acids (e.g., fatty acids) for HPLC analysis, please see one or more of the following three references:1. K.J. Longmuir, et al., Determination of monoenoic fatty acid double bond position by permanganate-periodate oxidation followed by high-performance liquid chromatography of carboxylic acid phenacyl esters. Analytical Biochemistry, 167(2), 213-221 (1987).2. T. Hanis et al., Determination of fatty acids as phenacyl esters in rat adipose tissue and blood vessel walls by high-performance liquid chromatography. Journal of Chromatography, 452, 443-457 (1988). 3. A. Mehta et al., Rapid quantitation of free fatty acids in human plasma by high-performance liquid chromatography. Journal of Chromatography B Biomedical Science Applications, 719(1-2), 9-23 (1998).
77450
2-Bromoacetophenone
derivatization grade (GC derivatization), LiChropur™, ≥99.0%
Synonym(s):
ω-Bromoacetophenone, Phenacyl bromide
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| Size/SKU | Availability | Price |
|---|---|---|
10 g | Estimated to ship TODAYfromMILWAUKEE | $216.00 $162.00 |
About This Item
$162.00
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grade
derivatization grade (GC derivatization)
Quality Segment
assay
≥99.0% (GC), ≥99.0%
form
crystals
quality
LiChropur™
reaction suitability
reagent type: derivatization reagent
reaction type: Acylations
technique(s)
gas chromatography (GC): suitable
bp
135 °C/18 mmHg (lit.)
mp
48-51 °C (lit.), 49-50 °C
storage temp.
2-8°C
SMILES string
BrCC(=O)c1ccccc1
InChI
1S/C8H7BrO/c9-6-8(10)7-4-2-1-3-5-7/h1-5H,6H2
InChI key
LIGACIXOYTUXAW-UHFFFAOYSA-N
General description
Application
Legal Information
1 of 1
This Item | |||
|---|---|---|---|
| description derivatization grade (GC derivatization), LiChropur™, ≥99.0% | description 98% | description >98% | description derivatization grade (HPLC), LiChropur™, ≥99.0% (HPLC) |
| assay ≥99.0% (GC) | assay 98% | assay >98% | assay ≥99.0% (HPLC) |
| Quality Level 100 | Quality Level 100 | Quality Level 200 | Quality Level 100 |
| reaction suitability reagent type: derivatization reagent | reaction suitability - | reaction suitability - | reaction suitability - |
| storage temp. 2-8°C | storage temp. - | storage temp. - | storage temp. - |
| mp 48-51 °C (lit.), 49-50 °C | mp 48-51 °C (lit.) | mp 108-110 °C (lit.) | mp 108-110 °C (lit.), 108-112 °C |
| form crystals | form solid | form crystals | form solid |
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signalword
Danger
Storage Class
6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials
flash_point_f
235.4 °F - closed cup
flash_point_c
113 °C - closed cup
ppe
Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges
hcodes
Hazard Classifications
Acute Tox. 4 Oral - Eye Dam. 1 - Skin Corr. 1B - Skin Sens. 1
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Do you have references on the use of 2-Bromoacetophenone (also known as phenacyl bromide) Products 115835 and 77450 for making phenacyl esters of carboxylic acids for HPLC analysis?
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Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.
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