C213630
Proligo Reagents
≥98% (31P-NMR)
≥98.0% (reversed phase HPLC)
solid
oligo synthesis: suitable
≤0.3 wt. % water content (Karl Fischer)
≤0.5% 3′-TC isomer (reversed phase HPLC)
≤0.5% P(III) Impurities 145-155ppm (31P-NMR)
white to light yellow
acetonitrile: toluene (1:1): 0.1 M at 18 °C, clear
conforms (UV/VIS Identity)
configured for ABI
base: cytidine
base protecting group: acetyl
2' protecting group: TC
5' protecting group: DMT
deprotection: fast
−20°C
COc1ccc(cc1)C(OC[C@H]2O[C@H]([C@H](OC(=S)N3CCS(=O)(=O)CC3)[C@@H]2OP(OCCC#N)N(C(C)C)C(C)C)N4C=CC(NC(C)=O)=NC4=O)(c5ccccc5)c6ccc(OC)cc6
1S/C46H57N6O11PS2/c1-31(2)52(32(3)4)64(60-27-11-23-47)63-41-39(30-59-46(34-12-9-8-10-13-34,35-14-18-37(57-6)19-15-35)36-16-20-38(58-7)21-17-36)61-43(51-24-22-40(48-33(5)53)49-44(51)54)42(41)62-45(65)50-25-28-66(55,56)29-26-50/h8-10,12-22,24,31-32,39,41-43H,11,25-30H2,1-7H3,(H,48,49,53,54)/t39-,41-,42-,43-,64?/m1/s1
OUGOPIOQANCAOY-JFALYFJISA-N
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13 - Non Combustible Solids
WGK 3
Not applicable
Not applicable
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