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MilliporeSigma

20724AST

Supelco

Astec® CYCLOBOND I 2000 DMP Chiral (5 μm) HPLC Columns

L × I.D. 25 cm × 4.6 mm, HPLC Column

Synonym(s):

TM=["CYCLOBOND"] I 2000 DMP Chiral HPLC Column

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About This Item

UNSPSC Code:
41115700
eCl@ss:
32110501
NACRES:
SB.52

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Product Name

Astec® CYCLOBOND I 2000 DMP Chiral HPLC Column, 5 μm particle size, L × I.D. 25 cm × 4.6 mm

material

stainless steel column

Quality Level

product line

Astec®

packaging

pkg of 1 ea

manufacturer/tradename

Astec®

parameter

0-50 °C temperature
172 bar pressure (2500 psi)

technique(s)

HPLC: suitable
LC/MS: suitable

L × I.D.

25 cm × 4.6 mm

matrix

silica particle platform
fully porous particle

matrix active group

cyclodextrin, beta- phase

particle size

5 μm

pore size

100 Å

operating pH

3.5-7

separation technique

chiral

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1 of 4

This Item
20734AST20744AST20324AST
particle size

5 μm

particle size

5 μm

particle size

5 μm

particle size

5 μm

L × I.D.

25 cm × 4.6 mm

L × I.D.

25 cm × 10 mm

L × I.D.

25 cm × 21.2 mm

L × I.D.

25 cm × 4.6 mm

separation technique

chiral

separation technique

chiral

separation technique

chiral

separation technique

chiral

matrix active group

cyclodextrin, beta- phase

matrix active group

cyclodextrin, beta- phase

matrix active group

cyclodextrin, beta- phase

matrix active group

cyclodextrin, beta- phase

matrix

silica particle platform, fully porous particle

matrix

silica particle platform, fully porous particle

matrix

silica particle platform, fully porous particle

matrix

silica particle platform, fully porous particle

product line

Astec®

product line

Astec®

product line

Astec®

product line

Astec®

General description

The reaction of the 3,5-dimethylphenyl isocyanate with the hydroxyl groups of β-cyclodextrin results in a pi-basic phase similar in character to the naphthylethyl carbamate phases. The selectivity is greater for the CYCLOBOND I 2000 DMP when the chiral center of the analyte is part of a ring structure or is on the α carbon. This phase has been very useful for derivatized amines, like amphetamine ACQ.

  • Bonded phase: 3,5-Dimethylphenyl carbamate modified β-cyclodextrin

Other Notes

Discover LiChropur reagents ideal for HPLC or LC-MS analysis

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany

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Rapid high-performance liquid chromatographic separation of barley malt a-amylase on cyclobond columns
Henson, Cynthia A., Stone, Julie M.
Journal of Chromatography A, 469, 361-367 (1989)
Indirect photodetection of pregnanolone on a Cyclobond column by high-performance liquid chromatography
Agnus, Benoit, et al.
Journal of Chromatography A, 633 (1), 27-33 (1994)
Reprint of: Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 968, 40-48 (2014)
Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 955-956, 72-80 (2014)
István Ilisz et al.
Chirality, 21(3), 339-348 (2008-06-17)
The application of 3,5-dimethylphenyl-carbamoylated-beta-cyclodextrin (Cyclobond I 2000 DMP) and 2,6-dinitro-4-trifluoromethylphenyl-ether-beta-cyclodextrin-based (Cyclobond DNP) chiral stationary phases for the high-performance liquid chromatographic enantioseparation of unusual beta-amino acids is reported. The investigated amino acids were saturated or unsaturated alicyclic beta-3-homo-amino acids and bicyclic

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