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24036

Supelco

SPB®-5 Capillary GC Column

L × I.D. 60 m × 0.25 mm, df 0.25 μm

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eCl@ss:
32119290

material

fused silica

Quality Level

100

Agency

meets requirements for USP G27 and G36

parameter

-60-320 °C temperature (isothermal or programmed)

Beta value

250

df

0.25 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

60 m × 0.25 mm

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

column type

capillary non-polar

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This Item
240372405124034
SPB®-5 Capillary GC Column L × I.D. 60 m × 0.25 mm, df 0.25 μm

Supelco

24036

SPB®-5 Capillary GC Column

SPB®-5 Capillary GC Column L × I.D. 60 m × 0.25 mm, df 1.00 μm

Supelco

24037

SPB®-5 Capillary GC Column

SPB®-5 Capillary GC Column L × I.D. 60 m × 0.32 mm, df 1.00 μm

Supelco

24051

SPB®-5 Capillary GC Column

SPB®-5 Capillary GC Column L × I.D. 30 m × 0.25 mm, df 0.25 μm

Supelco

24034

SPB®-5 Capillary GC Column

agency

meets requirements for USP G27 and G36

agency

meets requirements for USP G27 and G36

agency

meets requirements for USP G27 and G36

agency

meets requirements for USP G27 and G36

parameter

-60-320 °C temperature (isothermal or programmed)

parameter

-60-320 °C temperature (isothermal or programmed)

parameter

-60-320 °C temperature (isothermal or programmed)

parameter

-60-320 °C temperature (isothermal or programmed)

df

0.25 μm

df

1.00 μm

df

1.00 μm

df

0.25 μm

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

General description

Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded
  • Poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
  • ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)

Application

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may also be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. Furthermore, it may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SPB is a registered trademark of Sigma-Aldrich Co. LLC

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
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