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24241-U

Supelco

Carboxen®-1006 PLOT Capillary GC Column

L × I.D. 30 m × 0.32 mm, average thickness 15 μm

NACRES:
SB.54

material

fused silica

Quality Level

description

PLOT = Porous Layer Open Tubular

manufacturer/tradename

Carboxen®

parameter

≤25-250 °C temperature (isothermal or programmed)

average thickness

15 μm

df

15 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.32 mm

matrix active group

Carbon molecular sieve phase

application(s)

chemicals and industrial polymers
food and beverages

column type

capillary PLOT

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254612424625467
parameter

≤25-250 °C temperature (isothermal or programmed)

parameter

≤25-250 °C temperature (isothermal or programmed)

parameter

≤25-250 °C temperature (isothermal or programmed)

parameter

≤25-250 °C temperature (isothermal or programmed)

df

15 μm

df

30 μm

df

15 μm

df

30 μm

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

matrix active group

Carbon molecular sieve phase

matrix active group

Carbon molecular sieve phase

matrix active group

Carbon molecular sieve phase

matrix active group

Carbon molecular sieve phase

application(s)

chemicals and industrial polymers
food and beverages

application(s)

chemicals and industrial polymers
food and beverages

application(s)

chemicals and industrial polymers
food and beverages

application(s)

chemicals and industrial polymers
food and beverages

General description

Porous-layer open-tubular (PLOT) columns are a powerful tool used in gas chromatography for analysis of fixed gases, light hydrocarbons and volatile solvents. They are mostly preferred over traditional columns.
Application: This column is ideal for the separation of many permanent gas components (such as helium, hydrogen, nitrogen, carbon monoxide, methane, and carbon dioxide), and light hydrocarbons (C2-C3) in the same analysis. It is ideal for resolving formaldehyde/water/methanol (formalin) mixtures and monitoring impurities in ethylene. This column can be used with high flow rates and rapid temperature programs to ensure excellent, fast separations.
USP Code: None
Phase:
  • Carbon molecular sieve
Temp. Limits:
  • Subambient to 250 °C (isothermal or programmed)

Application

  • Carboxen® 1006 PLOT capillary column may be used as an extraction device in liquid chromatography-mass spectrometry (LC-MS) coupled with in-tube solid-phase microextraction, used in order to determine patulin in dried fruit samples and fruit juice.
  • Carboxen®-1006/polydimethylsiloxane(PDMS) fiber mounted in an SPME manual holder assembly coupled with GC-MS may be used for testing lipid oxidation products in milk.
  • It may also be used as an extraction device in liquid chromatography-mass spectrometry (LC-MS) coupled with in-tube solid-phase microextraction, in order to determine ochratoxins A and B in nuts and grain samples.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

Carboxen is a registered trademark of Sigma-Aldrich Co. LLC

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Porous layer open-tubular capillary columns: preparations, applications and future directions.
Journal of Chromatography A, 842 (1), 115-142 (1999)
R T Marsili
Journal of chromatographic science, 37(1), 17-23 (1999-02-13)
A sensitive, rapid procedure for testing lipid oxidation products in milk is developed using solid-phase microextraction (SPME) and gas chromatography-mass spectrometry. SPME is as sensitive as dynamic headspace (DH) analysis for measuring the pentanal and hexanal produced in milk after
H Kataoka et al.
Journal of chromatography. A, 1216(18), 3746-3750 (2009-03-25)
A simple and sensitive method for the determination of patulin in fruit juice and dried fruit samples was developed using a fully automated method consisting of in-tube solid-phase microextraction (SPME) coupled with liquid chromatography-mass spectrometry (LC-MS). Patulin was separated within
Dawn M Chapman et al.
Journal of agricultural and food chemistry, 52(17), 5431-5435 (2004-08-19)
A rapid and automated solid phase microextraction (SPME) stable isotope dilution gas chromatography/mass spectrometry (GC-MS) method for 2-methoxy-3-isobutylpyrazine (MIBP) quantification in red wine was developed. Wines with 30% (w/v) NaCl and 2-methoxy-(2)H(3)-3-isobutylpyrazine internal standard were sampled with a 2 cm
Lucia Giordano et al.
Journal of chromatography. A, 1017(1-2), 141-149 (2003-10-31)
A new method was developed for the determination of 2-furfural (2-F) and 5-methylfurfural (5-MF), two products of Maillard reaction in vinegar, with head-space solid-phase microextraction (HS-SPME) coupled to gas chromatography-mass spectrometry (GC-MS). A divinylbenzene (DVB)/carboxen (CAR)/polydimethylsiloxane (PDMS) fibre was used

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