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57051

Supelco

Supelclean LC-Si SPE Tube

bed wt. 1 g, volume 6 mL, pkg of 30 ea

material

PE frit
polypropylene hardware

Quality Level

product line

Supelclean

composition

bed wt., 1 g

packaging

pkg of 30 ea

technique(s)

solid phase extraction (SPE): suitable

surface area

475 m2/g

volume

6 mL

matrix

silica gel base material (irregularly shaped)

matrix active group

silica bonding

particle size

45 μm

pore size

0.8 cm3/g pore volume
60 Å pore size

application(s)

food and beverages

separation technique

normal phase

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This Item
5040415711657133
Supelco

Supelco

57051

Supelclean LC-Si SPE Tube

Supelclean™ LC-Si SPE Tube bed wt. 2 g, volume 12 mL, pk of 20

Supelco

57116

Supelclean LC-Si SPE Tube

Supelco

Supelco

57133

Supelclean LC-Si SPE Tube

composition

bed wt., 1 g

composition

bed wt., 100 mg

composition

bed wt., 2 g

composition

bed wt., 5 g

packaging

pkg of 30 ea

packaging

pk of 108

packaging

pk of 20

packaging

pk of 20

volume

6 mL

volume

1 mL

volume

12 mL

volume

20 mL

matrix

silica gel base material (irregularly shaped)

matrix

silica gel base material (irregularly shaped)

matrix

silica gel base material (irregularly shaped)

matrix

silica gel base material (irregularly shaped)

matrix active group

silica bonding

matrix active group

silica bonding

matrix active group

silica bonding

matrix active group

silica bonding

General description

Supelclean LC-Si SPE tube is used to extract polar analytes from nonpolar samples.

Application

Supelclean LC-Si SPE Tube may be used for the solid-phase extraction of:
  • Phospholipids in dairy products prior to their determination by high performance liquid chromatography-evaporative light scattering detector (HPLC-ELSD).
  • Free and esterified sterols in Portuguese olive oils prior to their estimation by gas chromatography-mass spectrometry (GC-MS).
  • Synthetic musks in cream prior to their quantification by GC combined with tandem mass spectrometry (MS/MS).
  • Phospholipids in milk samples prior to their quantification by hydrophilic interaction liquid chromatography (HILIC) in conjunction with ELSD as well as ion trap-time-of-flight mass spectrometry (IT-TOF MS).

Legal Information

Supelclean is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

11 - Combustible Solids

WGK

nwg

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


Certificates of Analysis (COA)

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T1503
Product Number
-
25G
Pack Size/Quantity

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705578-5MG-PW

PL860-CGA/SHF-1EA

MMYOMAG-74K-13

1000309185

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Customers Also Viewed

Analysis of 7 synthetic musks in cream by supported liquid extraction and solid phase extraction followed by GC-MS/MS.
Dong H, et al.
Talanta, 120(1-2), 248-254 (2014)
Quantification of free and esterified sterols in Portuguese olive oils by solid-phase extraction and gas chromatography-mass spectrometry.
Cunha SS, et al.
Journal of Chromatography A, 1128(1-2), 220-227 (2006)
Determination of phospholipids in milk samples by means of hydrophilic interaction liquid chromatography coupled to evaporative light scattering and mass spectrometry detection.
Donato P, et al.
Journal of Chromatography A, 1218(37), 6476-6482 (2011)
Determination of phospholipids in dairy products by SPE/HPLC/ELSD.
Avalli A and Contarini G
Journal of Chromatography A, 1071(1-2), 185-190 (2005)

Protocols

LC/MS Analysis of Phospholipids in Milk on Ascentis® Express HILIC after SPE using Supelclean Si, Shotgun HPLC Analysis

(soybean), ≥97%; L-α-Phosphatidylethanolamine from egg yolk, Type III, ≥97% (TLC), lyophilized powder; L-α-Phosphatidylcholine, from egg yolk, Type XVI-E, ≥99% (TLC), lyophilized powder; Sphingomyelin, from chicken egg yolk, ≥95%

Chromatograms

suitable for GC, application for SPE

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