MilliporeSigma
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57439-U

Supelco

SPME-OC Fiber Assembly, Polydimethylsiloxane/Divinylbenzene (PDMS/DVB)

df 75 μm (Coating thickness includes 65 μm coating + 10 μm OC (overcoating)), needle size 23 ga, pkg of 3 ea, fiber L 1 cm

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Synonym(s):
SPME-Overcoated Fiber Polydimethylsiloxane/Divinylbenzene (PDMS/DVB)
NACRES:
NB.21

Quality Level

100

material

StableFlex fiber (Polydimethylsiloxane/Divinylbenzene (PDMS/DVB))
notched pink hub

needle size

23 ga

description

Polydimethylsiloxane/Divinylbenzene (PDMS/DVB) fiber overcoated with a layer of PDMS.

packaging

pkg of 3 ea

df

75 μm (Coating thickness includes 65 μm coating + 10 μm OC (overcoating))

technique(s)

solid phase microextraction (SPME): suitable

fiber L

1 cm

matrix active group

PDMS/DVB coating, Overcoated Polydimethylsiloxane/Divinylbenzene

application(s)

food and beverages

compatibility

for use with autosampler or manual (for direct immersion into matrix or headspace analysis of volatile or semi-volatile analytes (MW 50-300+))

Related Categories

General description

A new development in SPME fiber technology incorporates a protective overcoating on the fiber. This overcoating, which consists of polydimethylsiloxane (PDMS) serves as a barrier to protect the fiber from the matrix, which makes it more physically robust and less prone to chemical fouling. High background samples, such as many foods, pose a challenge to immersion SPME due to the presence of fats, sugars, pigments, and other macromolecules. These can stick to the SPME fiber and reduce its usable life and/or be transferred to the GC, where they may interfere with chromatographic analysis. Overcoating the fiber with PDMS reduces these problems.

Certificate of Analysis

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Certificate of Origin

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Esther De La Fuente et al.
Journal of environmental science and health. Part A, Toxic/hazardous substances & environmental engineering, 44(10), 1004-1010 (2009-10-16)
The complex molecular assemblages were analysed in the soil gas phase after applying pine forest wastes (PFW) or sugarbeet vinasses (SBV) for soil-borne crop pests' management. For this purpose, solid-phase micro-extraction (SPME) and gas chromatography (GC) were used coupled with
Marghereth Saverini et al.
Journal of photochemistry and photobiology. B, Biology, 108, 8-15 (2012-01-20)
The presence of (±)α-pinene, (+)β-pinene, (+)3-carene, and R-(+)limonene terpenes in wastewater of a citrus transformation factory was detected and analyzed, in a previous study, by using Solid Phase Micro-extraction (SPME) followed by GC analyses. Purpose of that research was to
M A Stack et al.
Chemosphere, 41(11), 1821-1826 (2000-11-01)
Solid phase micro extraction (SPME) was applied to the determination of selected trihalomethanes (THMs), chloroform, bromodichloromethane, dibromochloromethane, bromoform, in potable and recreational waters. The selected samples were environmentally significant due to mandatory limits imposed by regulatory agencies. Extraction of the
Mona Syhre et al.
Tuberculosis (Edinburgh, Scotland), 88(4), 317-323 (2008-02-26)
Worldwide, tuberculosis (TB) kills nearly 2 million people annually, yet rapid diagnosis still relies on a 100-year-old method of sputum staining for acid-fast bacilli. The advent of solid phase micro-extraction and gas chromatography/mass spectrometry makes it possible to systematically investigate
Gustavo Charry-Parra et al.
Journal of food science, 76(2), C205-C211 (2011-05-04)
A powerful technique was developed for the identification and quantification of 9 volatile compounds of beer, using headspace solid phase micro-extraction (HS/SPME) and gas chromatograph coupled to a mass spectrometer and a flame ionization detector (GC/MS/FID). Optimized parameters included type
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Articles

Analysis of Pesticides in Baby Food by Solid Phase Microextraction (SPME) Using a New Overcoated Fiber

A direct immersion SPME method using a new overcoated SPME fiber was developed for the extraction of pesticides from pureed prune baby food.

GC/MS/MS Analysis of Bisphenol A (BPA) in a Fruit Flavored Energy Drink on the SLB-PAHms Column After SPME Using an Overcoated SPME Fiber

Bisphenol A (BPA) plastic is controversial in food and beverage containers. This study demonstrates SPME of BPA from an energy drink using an overcoated PDMS/DVB fiber, followed by GC/MS/MS analysis using SLB-PAHms GC Column.

Multiclass Pesticide Analysis of Soy Milk Using a Matrix-Compatible SPME Fiber

Pesticide analysis, SPME Fiber, supelco spme fiber, direct immersion spme, pesticide analysis methods, pesticide analysis by gc-ms, DI-SPME, overcoated SPME, overcoated fibers, soy milk analysis

Protocols

Analysis of Bisphenol A in Food by Solid Phase Microextraction Using an Overcoated Fiber

Bisphenol A (BPA) is suspected to be an endocrine disruptor. Regulations on specific migration limits (SML) from food contact materials are getting tighter (EU 2018/213) requiring more sensitive determinations. An overcoated SPME fiber provides the durability necessary for direct immersion into foods such as canned soup and pumpkin, allowing for low level analysis of BPA via SPME-GC-MS/MS.

Related Content

Solid Phase Microextraction (SPME)

Solid phase microextraction (SPME) is a solvent-free sample preparation technique that uses coated fibers to extract analytes of interest from a sample before analysis by GC or HPLC.

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