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José Fernando Huertas-Pérez et al.
Journal of pharmaceutical and biomedical analysis, 124, 261-266 (2016-03-13)
A simple, effective and reliable method for the determination of eight sulfonamide antibiotics (sulfadiazine, sulfapiridine, sulfamerazine, sulfamethazine, sulfachloropiridazine, sulfamethoxazole, sulfadoxine, sulfadimethoxin) in chicken muscle and eggs by liquid chromatography and fluorescence detection has been developed and validated. Sulfonamides do not
Martina Rejtharová et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 35(2), 233-240 (2017-10-06)
A sensitive and robust confirmatory method for determination of steroid esters in blood serum is essential for reliable monitoring of possible illegal use of steroid hormones as growth promoters in meat production. A previously used sample preparation methodology was improved.
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction
P Parrilla Vázquez et al.
Journal of chromatography. A, 1463, 20-31 (2016-08-18)
The aim of this research was to adapt the QuEChERS method for routine pesticide multiresidue analysis in edible vegetable oil samples using gas chromatography coupled to tandem mass spectrometry (GC-MS/MS). Several clean-up approaches were tested: (a) D-SPE with Enhanced Matrix
Giorgia Purcaro et al.
Journal of chromatography. A, 1307, 166-171 (2013-08-07)
The aim of the present work was to optimize a preparation step for polycyclic aromatic hydrocarbons in a fatty extract. Solid-phase microextraction is an easy preparation technique, which allows to minimize solvent consumption and reduce sample manipulation. A Carbopack Z/polydimethylsiloxane
Piotr Kaczyński et al.
Ecotoxicology and environmental safety, 138, 179-189 (2017-01-06)
The analysis of pesticide residues in fish samples is challenging due to the low concentrations and large number of analytes that need to be monitored and quantified in a complex matrix. This is the first report providing a novel one-step
Ana Lozano et al.
Talanta, 118, 68-83 (2013-11-28)
Two sorbents containing ZrO₂ (Z-Sep and Z-Sep+) were tested as a d-SPE clean-up in combination with the QuEChERS and ethyl acetate multiresidue method in the pesticide residues extraction in avocado. All extracts were analysed using gas chromatography coupled with a
Edouard Lehmann et al.
Analytica chimica acta, 999, 87-98 (2017-12-20)
The present study assessed the suitability of using QuEChERS procedure for the simultaneous determination and quantification of 37 multi-class pesticides in human hair. Matrix co-eluted material had a large influence on instrumental response sensitivity. Purification was needed although dSPE cleanup
Yin-E Liu et al.
Journal of chromatography. A, 1532, 68-73 (2017-12-13)
An analytical method has been developed for measuring 12 organophosphorus flame retardants (PFRs) in fish tissue samples. After the Soxhlet extraction of PFRs with dichloromethane. The experimental parameters of the clean-up were systematically optimized. Methanol was found to be a
Multi-pesticide residue analysis in nutraceuticals from grape seed extracts by gas chromatography coupled to triple quadrupole mass spectrometry
Nieto-Garcia, A.J., et al.
Food Control, 47, 369-380 (2015)
Piotr Kaczynski et al.
Ecotoxicology and environmental safety, 139, 124-131 (2017-01-28)
Highly toxic insecticides (HTIs) belonging to different chemical groups are dangerous to pollinating organisms, even in sublethal doses. An important objective of this study was to develop a method to determine over fifty HTIs at very low concentrations in the
Yuanbo Li et al.
Talanta, 140, 81-87 (2015-06-07)
One of the hypotheses that may help explain the loss of honey bee colonies worldwide is the increasing potential for exposure of honey bees to complex mixtures of pesticides. To better understand this phenomenon, two multi-residue methods based on different
Stanisław Walorczyk et al.
Journal of chromatography. A, 1412, 22-32 (2015-08-25)
Two-step dispersive-solid phase extraction strategy for the cleanup of QuEChERS extracts in multiresidue analysis of current-use pesticides in a chlorophyll-containing matrix was evaluated and is reported for the first time. The proposed approach combines two sequential steps of dispersive-solid phase
Bruce D Morris et al.
Journal of agricultural and food chemistry, 63(21), 5107-5119 (2015-02-24)
A new, automated, high-throughput, mini-column solid-phase extraction (c-SPE) cleanup method for QuEChERS extracts was developed, using a robotic X-Y-Z instrument autosampler, for analysis of pesticide residues in fruits and vegetables by LC-MS/MS. Removal of avocado matrix and recoveries of 263
Jonatan V Dias et al.
Journal of chromatography. A, 1462, 8-18 (2016-08-11)
The goal of this work was to evaluate the efficiency of several sorbents on removal fats from edible oils (olive, soya and sunflower) during the clean-up step for posterior determination of 165 pesticides by UHPLC-QqQ-MS/MS system. The extraction procedure employed
Rafael López-Blanco et al.
Journal of chromatography. A, 1456, 89-104 (2016-06-23)
In this article we have evaluated the performance of different sorbents for the cleanup step in multiresidue pesticide analysis in fatty vegetable matrices using QuEChERS methodology. The three different matrices tested (olive oil, olives and avocado) were partitioned using acetonitrile
P Parrilla Vázquez et al.
Journal of chromatography. A, 1426, 161-173 (2015-12-15)
Several clean-up methods were evaluated for 253 pesticides in pollen samples concentrating on efficient clean-up and the highest number of pesticides satisfying the recovery and precision criteria. These were: (a) modified QuEChERS using dSPE with PSA+C18; (b) freeze-out prior to
Ahmed M Hamed et al.
Journal of separation science, 40(2), 488-496 (2016-11-20)
A simple and efficient method for the determination of 28 carbamates in high-fat cheeses is proposed. The methodology is based on a modified quick, easy, cheap, effective, rugged, and safe procedure as sample treatment using a new sorbent (Z-Sep
M Picot Groz et al.
The Science of the total environment, 493, 162-169 (2014-06-20)
The UV filters and musk fragrances have come into focus because these compounds are contained and increasingly used not only in sunscreen products but also in many products of daily use, such as cosmetics, skin creams, plastics or varnish. In
J A Custodio-Mendoza et al.
Journal of chromatography. A, 1548, 19-26 (2018-03-21)
A fast and effective method using a modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) approach which includes partitioned liquid-liquid extraction (PLLE) and dispersive solid phase extraction (dSPE) clean-up step for the determination of seven 3-monochloropropane-1,2-diol (3-MCPD) fatty acid
Tomasz Kiljanek et al.
Journal of chromatography. A, 1435, 100-114 (2016-02-03)
A method for the determination of 200 pesticides and pesticide metabolites in honeybee samples has been developed and validated. Almost 98% of compounds included in this method are approved to use within European Union, as active substances of plant protection
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using
An overview of analytical methods and occurrence of benzotriazoles, benzothiazoles and benzenesulfonamides in the environment
Herrero, P., et al.
TrAC, Trends in Analytical Chemistry, 62, 46-55 (2014)
Keiko Iwakoshi et al.
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 57(5), 150-154 (2016-10-28)
Rapid multi-residue analysis of pesticides in pulses was developed using LC-MS/MS. Pesticide residues in 5 g of homogenized pulses were extracted with 30 mL of acetonitrile and salted out with 4 g of anhydrous magnesium sulfate and 2 g of
David Moreno-González et al.
Talanta, 128, 299-304 (2014-07-26)
In this study a fast, selective and sensitive multiresidue method based on QuEChERS methodology has been evaluated and validated for the determination of carbamate pesticides, in edible vegetable oils by UHPLC-MS/MS. A new clean-up sorbent, Supel(TM) QuE Z-Sep(+), has been
Łukasz Rajski et al.
Journal of chromatography. A, 1304, 109-120 (2013-07-23)
Several extraction methods were evaluated in terms of recoveries and extraction precision for 113 pesticides in avocado: QuEChERS with various d-SPE clean-ups (Z-Sep, Z-Sep+, PSA+C18 and silica), miniLuke and ethyl acetate. Extracts were analysed using liquid chromatography coupled with triple
Tomasz Tuzimski et al.
Journal of AOAC International, 100(6), 1671-1680 (2017-07-15)
In this study, a simple, cost-effective, and sensitive HPLC diode-array detection method was developed for the simultaneous determination of six different 5-nitroimidazoles [metronidazole, 2-hydroxymethyl-1-methyl-5-nitro-1H-imidazole, dimetridazole (DMZ), ronidazole, ornidazole, and ipronidazole] in bovine milk samples. A QuEChERS-based sample preparation procedure was
Lijun Han et al.
Journal of separation science, 39(23), 4592-4602 (2016-11-03)
A novel carbon/zirconia-based material, Supel
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Hui Li et al.
Journal of chromatography. A, 1528, 53-60 (2017-11-07)
Herein, an accurate and reliable isotope-labelled internal standard method was developed and validated for simultaneous determination of three polar pesticide adjuvants, namely 2-pyrrolidone, N-methyl-2-pyrrolidone, and N-ethyl-2-pyrrolidone in plant-derived agro-products. Matrices, including apple, cabbage, tomato, cucumber, rice, and wheat were extracted
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