MilliporeSigma
Search Within
Applications
Content Type
Collections

Solid phase extraction

Applied Filters:
facet applications:Solid phase extraction
facet content type:Protocol
LC/MS Analysis of Phospholipids in Milk on Ascentis® Express HILIC after SPE using Supelclean Si, Shotgun HPLC Analysis
(soybean), ≥97%; L-α-Phosphatidylethanolamine from egg yolk, Type III, ≥97% (TLC), lyophilized powder; L-α-Phosphatidylcholine, from egg yolk, Type XVI-E, ≥99% (TLC), lyophilized powder; Sphingomyelin, from chicken egg yolk, ≥95%
ENVI-Carb Plus for the Extraction of Propylene Glycol and Ethylene Glycol from Water
ENVI-Carb Plus for the Extraction of Propylene Glycol and Ethylene Glycol from Water
Using UHPLC/MS (TOF) for Detection of Drugs and Metabolites in Urine Following Optimized Enzymatic Hydrolysis Conditions
To optimize hydrolysis using β-glucuronidase, factors such as incubation time, temperature, hydrolysis pH, enzyme source, and enzyme concentration must be evaluated for each glucuronide metabolite to be analyzed.
Selective Extraction and Cleanup of Patulin Mycotoxin from Apple Juice Samples
This selective and fast MIP extraction procedure allows trace amounts of patulin to be easily detected in apple juice, with high analyte recovery and reproducibility.
Acrylamide in Food
Acrylamide analysis has been a very hot topic since the chemical was identified in food in 2002 by researchers at the Swedish National Food Administration.
LC/MS Analysis of Opioid Glucuronide Metabolites in Urine on Ascentis® Express F5 after Solid Phase Extraction (SPE) using Supel™-Select HLB
LC/MS Analysis of Opioid Glucuronide Metabolites in Urine on Ascentis® Express F5 after Solid Phase Extraction (SPE) using Supel™-Select HLB
Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS
Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS
Fraction of cis/trans FAMEs Using Discovery® Ag-Ion SPE
Fraction of cis/trans FAMEs Using Discovery® Ag-Ion SPE
LC/MS/MS Analysis of Interacting Cardiac Drugs Digoxin, Quinidine, Amiodarone and Verapamil on Titan™ C18
LC/MS/MS Analysis of Interacting Cardiac Drugs Digoxin, Quinidine, Amiodarone and Verapamil on Titan™ C18
Empowering Biochemists to Analyze Glycoproteins with Exceptional Reproducibility
Fast, high-resolution separations of procainamide labeled glycans - dextran ladder, human IgG and cetuximab
Determination of Triclosan in Environmental Waters
Triclosan was detected in waste water plant discharge using HPLC followed by UV and MS/MS detection.
Determination of Bisphenol A in Drinking Water
A comprehensive sample preparation and analytical procedure was developed by Supelco for determining BPA in drinking water.
Accurate Biological Testing for Amphetamine and Methamphetamine Abuse Using Chiral HPLC and MS Detection
Optimized sample prep and chiral chromatography methods for the LC/MS analysis of these drug enantiomers in urine
Online SPE/LC-MS Method for the Rapid Analysis of Thyroid Hormones in Plasma
Determination of the thyroid hormones T4, T3 and rT3 from plasma using an Ascentis Express RP-Amide cartridge to trap the analytes, and a Phenyl-Hexyl column to resolve them.
Solid Phase Extraction: Normal Phase Methodology
Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.
GC Analysis of Phenols in Water on a 5% Phenyl Column after SPE using Supelclean™ ENVI-Chrom P
Separation of 2-Nitrophenol; Pentachlorophenol; 2-Bromophenol; Phenol; 4-Nitrophenol; 3-Methylphenol, analytical standard; 4-Chloro-3-methylphenol; 2,4-Dichlorophenol; 2,3,4,6-Tetrachlorophenol; 2-Methylphenol, analytical standard; 2,4,6-Trichlorophenol; 2,4-Dimethylphenol; 2-Chlorophenol
Extraction and Analysis of Lasix (Furosemide) in Horse Serum
Studies have suggested that there is a correlation between furosemide and improved racing performance, prompting the horse racing industry to monitor the use of this drug
Biological Testing for Amphetamine and Methamphetamine Abuse
In this study, optimized methods are presented for sample preparation and chiral chromatography for the LC/MS analysis of amphetamine and methamphetamine enantiomers in urine.
Reversed-Phase SPE Methodology
Reversed-Phase SPE Methodology in Solid Phase Extraction. Reversed-phase SPE is considered the least selective retention mechanism when compared to normalphase or ion-exchange SPE.
LC/MS/MS Analysis of Aflatoxins in Hops on Ascentis® Express 2.7 μm Phenyl-Hexyl after Cleanup Using Supel™ Tox AflaZea SPE
LC/MS/MS Analysis of Aflatoxins in Hops on Ascentis® Express 2.7 μm Phenyl-Hexyl after Cleanup Using Supel™ Tox AflaZea SPE
Veterinary Drug Residues
The use of veterinary drugs may be integral to the process of raising food producing animals and fish. These can include antibiotics, hormones, and steroids.
Analysis of Melamine in Milk
Melamine was extracted from milk using Supelco® Discovery® DSC-SCX SPE tubes. Analysis was performed by HPLC, using an Ascentis® Express HILIC column.
Rapid, Sensitive, and Quantitative LC/MS/MS Determination of Digitoxin and Digoxin in Plasma
Immunoassay-based methods for digitoxin or digoxin exist, but are time consuming, labor intensive, and not selective due to similarities in their chemical structures.
LC/MS/MS Analysis of Steroid Hormones in Plasma
The conversion of clinical methods to LC/MS/MS offers advantages; however, is accompanied by a few limitations, notably interference effects from the endogenous sample matrix.
Determination of PAHs in Paprika Powder Using a Novel SPE Cartridge
Paprika is a spice made from dried sweet peppers, and is used for flavor and color in many types of cuisine. Contamination with polynuclear aromatic hydrocarbons (PAHs) can occur when pepper plants are exposed to these pollutants in the environment
Controlling SPE Selectivity Through pH and Organic Modifier Manipulation
Controlling SPE Selectivity Through pH and Organic Modifier Manipulation
Enrichment of Phospholipids in Biological Samples Using HybridSPE-PL
A simple method to enrich phospholipids from plasma samples, involving a HybridSPE-PPT 96-well plate that both retains phospholipids and removes precipitated proteins.
Page 1 of 2