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Metabolism of 5-methyl-2-furaldehyde in rat. III. Identification and determination of 5-methyl-2-furylmethylketone.

Xenobiotica; the fate of foreign compounds in biological systems (1988-08-01)
J Jodynis-Liebert
ABSTRACT

1. Continuous extraction, column chromatography and t.l.c. were employed to isolate a minor metabolite of 5-methyl-2-furaldehyde from rat urine. 2. The metabolite was identified by mass spectrometry and independent synthesis as 5-methyl-2-furylmethylketone. 3. A method for quantitative determination of the metabolite in urine was devised. About 7% of the parent compound was metabolized to 5-methyl-2-furylmethylketone.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
5-Methylfurfural, ReagentPlus®, 99%
Sigma-Aldrich
5-Methylfurfural, ≥98%, FG
Sigma-Aldrich
2-Acetyl-5-methylfuran, 98%
Sigma-Aldrich
2-Acetyl-5-methylfuran, ≥98%, FG

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