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US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms

US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms suitable for GC

Materials

analytical column

Product No.
Description
Pricing

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.50 μm

SLB®-5ms Capillary GC Column

L × I.D. 20 m × 0.18 mm, df 0.18 μm

Related product

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ORBO 2000 Precleaned Large PUF Cartridge

O.D. × L 6 cm × 7.6 cm, pkg of 1 ea

Glass Cartridge and Screen for Large PUF Plug

pkg of 1 ea

Stainless Steel Screen

ORBO 2000 Precleaned Large PUF Plug, Replacement

O.D. × L 6 cm × 7.6 cm, pkg of 1 ea

Supelpak-2

matrix styrene-divinylbenzene, 20-60 mesh, jar of 100 g

Inlet Liner, Split/Splitless Type, Straight Fast FocusLiner Design (wool packed)

pkg of 1 ea

accessory

Product No.
Description
Pricing

Supeltex M-2B Double-Tapered Ferrule

I.D. 0.4 mm, 0.10-0.25 mm to like I.D. Column, pkg of 2 ea

Capillary Column Butt Connector

body only (ferrules not included)

guard column

Product No.
Description
Pricing

Intermediate Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

standard

Product No.
Description
Pricing

Coronene

purified by sublimation, 99%

Benzo[e]pyrene

analytical standard

Perfluorotributylamine (PFTBA)

analytical standard

EPA 8270 GC-MS Tuning Solution II

certified reference material, 1000 μg/mL each component in dichloromethane

Perylene solution

certified reference material, 2000 μg/mL in dichloromethane

ORBO 2500 Precleaned Large PUF/Amberlite XAD®-2/PUF Cartridge

O.D. × L 6.5 cm × 125 mm, pkg of 1 ea

EPA 8270 Semivolatile Internal Standard Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mL

Polynuclear Aromatic Hydrocarbons Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride: benzene (1:1)

EPA 610 Polynuclear Aromatic Hydrocarbons Mix

certified reference material, in methanol: methylene chloride (1:1) (varied concentration)

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

60 °C (1 min), 10 °C/min to 340 °C (5 min)

inj. temp.

250 °C

MSD interface

330 °C 300 °C / 200 °C (source/quads)

scan range

m/z 40-450

carrier gas

helium, 1.5 mL/min. constant

injection

1.5 μL, pulsed (25 psi until 0.2 min) splitless (0.75 min)

liner

2 mm I.D. FocusLiner liner (2879601-U)

sample

22 component TO-13 standard plus 5 internal standards at 500 ppb in hexane:ethyl ether (90:10)

Description

Legal Information

FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany