US EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on Equity®-5 (30 m x 0.25 mm I.D., 0.50 μm)

Conditions

column Equity-5, 30 m x 0.25 mm I.D., 0.5 µm (28092-U)
oven 40 °C (2 min), 50 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (7.5 min)
carrier gas helium, pressure programmed, 20 psi (0.0 min), ramp to 80 psi (0.0 min), ramp to 16.5 psi (3 min), ramp to 25 psi (hold for remainder of run)
sample 50 ng on-column of a 62 Supplemental Appendix IX list consisting of semivolatile standards, 6 internal standards, and 8 surrogates
injection 1 µL, splitless (0.61 min)
liner 4 mm I.D., single taper
inj. temp. 280 °C, splitless (0.61 min)
detector MSD, Scan range 45-450 amu, 325C

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information Equity is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,2,4,5-Tetrachlorobenzene
  • 1,2-Dichlorobenzene-d4
  • 1,3,5-Trinitrobenzene
  • 1,3-Dinitrobenzene
  • 1,4-Dichlorobenzene-d4
  • 1,4-Dinitrobenzene
  • 1,4-Dioxane
  • 1,4-Naphthoquinone
  • 1-Methylnaphthalene
  • 1-Naphthylamine
  • 2,3,4,6-Tetrachlorophenol
  • 2,3,5,6-Tetrachlorophenol
  • 2,4,6-Tribromophenol
  • 2,6-Dichlorophenol
  • 2-Acetylaminofluorene
  • 2-Chlorophenol-d4
  • 2-Fluorobiphenyl
  • 2-Fluorophenol
  • 2-Naphthylamine
  • 2-Picoline
  • 3-Methylcholanthrene
  • 3-Methylphenol
  • 4-Aminobiphenyl
  • 4-Dimethylaminoazobenzene
  • 4-Nitroquinoline-1-oxide
  • 5-Nitro-o-toluidine
  • 7,12-Dimethylbenz[a]anthracene
  • Acenaphthene-d10
  • Acetophenone
  • Aniline
  • Benzyl alcohol
  • Chlorobenzilate
  • Chrysene-d12
  • Dialate-1
  • Dialate-2
  • Dibenzo[a,j]acridine
  • Dimethoate
  • Dinoseb
  • Diphenylamine
  • Disulfoton
  • Ethyl methanesulfonate
  • Famphur
  • Hexachloropropene-1
  • Isodrin
  • Isosafrole
  • Isosafrole-2
  • Kepone
  • Methapyrilene
  • Methyl methanesulfonate
  • Methyl parathion
  • Naphthalene-d8
  • Nitrobenzene-d5
  • N-Nitrosodibutylamine
  • N-Nitrosodiethylamine
  • N-Nitrosomerpholine
  • N-Nitrosomethylethylamine
  • N-Nitrosopiperidine
  • N-Nitrosopyrrolidine
  • o,o,o-Triethyl phosphorothioate
  • o-Toluidine
  • Parathion
  • Pentachlorobenzene
  • Pentachloroethane
  • Pentachloronitrobenzene
  • Perylene-d12
  • Phenacetin
  • Phenanthrene-d10
  • Phenol-d6
  • Phenylenediamine
  • Phorate
  • Pronamide
  • p-Terphenyl-d14
  • Pyridine
  • Safrole
  • Sulfotep
  • Thionazin
  • α,α-Dimethylphenethylamine
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