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Organic letters

Solid-phase synthesis of 1,7-disubstituted-1,3,5-triazepane-2,4-diones.


PMID 11529759

Abstract

[reaction: see text]. The solid-phase synthesis of 1,7-disubstituted-1,3,5-triazepane-2,4-diones from resin-bound amino acids is described. The exhaustive reduction of solid-support bound amides with borane afforded the requisite secondary amines, which following treatment with phenyl isocyanatoformate and cleavage, provided the corresponding triazepane-2,4-diones.

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478423
Phenyl isocyanatoformate, 97%
C8H5NO3